Ink Printing method utilizing stabilized polymeric particles
A polymer particle, polymer technology, applied in the field of ink printing, can solve problems such as ink difference stability, and achieve the effect of enhanced dye stability and good image quality
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Embodiment 1
[0131] Synthesis Example 1. Synthesis of Dispersant 1
[0132] Acrylamide (35.50 g, 0.50 mol) and 1-dodecanethiol (10.10 g, 0.050 mol) were suspended in ethanol (250 ml) in a 1 L three-neck round bottom flask equipped with a reflux condenser under nitrogen atmosphere . The solution was stirred and degassed with nitrogen for 20 minutes. Stirring was continued and the temperature was raised to 70°C over a period of 20 minutes during which time the reagents dissolved. 2,2′-Azo-bis(2-methylpropionitrile)[AIBN] (1.00 g, 6.10 mmol) was added to the stirred solution at 70° C., and heating was continued under the control of the automated reactor system 4 hours. During this time, a white suspension formed. After cooling, the obtained white precipitate was filtered under suction and dried under vacuum to give a white powder (39.6 g, 87%). Analysis of this product was consistent with the desired product.
Embodiment 2
[0133] Synthesis Example 2. Synthesis of Dispersant 2
[0134] Dispersant 2 was synthesized by using the same procedure as Dispersant 1, except that a higher molar ratio of acrylamide to dodecanethiol (20:1) was used.
Embodiment 3
[0135] Synthesis Example 3. Synthesis of Dispersant 3
[0136] N-acryloyltris(hydroxymethyl)aminomethane (52.5g, 0.40mol), hexadecylmercaptan (5.20g, 0.20mol), and AIBN (0.20g) were added to methanol (100ml) in 3 necked flask. The reaction was degassed by bubbling argon for 20 minutes and heated at reflux under an atmosphere of argon for 6 hours. After cooling, a sticky, white mass formed in the solution. The methanol was decanted off and the product redissolved in water. Freeze drying gave a white solid (40.5 g, 70%).
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