Catalytic and thermal cracking catalyst for increasing production of ethane and propylene
A catalytic thermal cracking and catalyst technology, applied in catalytic cracking, cracking, petroleum industry and other directions, can solve the problem that macromolecular catalytic reaction cannot be used, and achieve the effect of reducing coke and facilitating diffusion
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example 8
[0038] Example 8 illustrates the preparation process of the mesoporous silica-alumina material.
example 1
[0040] 20gNH 4 Cl was dissolved in 1000g of water, and 100g (dry basis) of the crystallized product ZRP zeolite (produced by Qilu Petrochemical Catalyst Factory, SiO2) was added to the solution. 2 / Al 2 O 3 =30, rare earth content RE 2 O 3 = 2.0 wt%), exchanged at 90 °C for 0.5 h, filtered to obtain a filter cake; added 4.2 gH 3 PO 4 (concentration 85%) with 4.8g Fe (NO 3 ) 3 Dissolved in 90 g of water, mixed with filter cake, dipped and dried; the obtained sample was calcined at 550°C for 2 hours. Its elemental analytical chemical composition is
[0041] 0.1Na 2 O 5.0Al 2 O 3 ·2.4P 2 O 5 1.5Fe 2 O 3 1.9RE 2 O 3 ·89.1SiO 2 .
example 2
[0043] 50gNH 4 Cl was dissolved in 1000g of water, and 100g (dry basis) of the crystallized product ZRP zeolite (produced by Qilu Petrochemical Catalyst Factory, SiO2) was added to the solution. 2 / Al 2 O 3 =30, rare earth content RE 2 O 3 = 2.0 wt%), after exchanged at 85°C for 0.5 h, the filter cake was obtained by filtration; 8.0 g NH 4 H 2 PO 4 Dissolved in 60 g of water, mixed with filter cake, dipped and dried, and calcined at 550 ° C for 2 hours; 3 ) 3 The solution was exchanged at 80-90°C for 2 hours, filtered, exchanged several times until the target amount was reached, and then calcined at 550°C for 2 hours. The chemical composition of elemental analysis is
[0044] 0.03Na 2 O 4.8Al 2 O 3 ·4.5P 2 O 5 ·3.0Fe 2 O 3 ·1.8RE 2 O 3 ·85.9SiO 2 .
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