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Process for preparing bamboo-based activated carbon and dedicated device therefor

A technology of activated carbon and bamboo, which is applied in the field of preparation of bamboo activated carbon, can solve the problems of difficulty in guaranteeing the uniformity and stability of product quality, no specific description of equipment, and large differences, etc. The effect of high production efficiency

Inactive Publication Date: 2006-12-27
浙江恒日炭业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

It can be seen that the position of the material is also fixed, so there are also large differences in the heating conditions of the materials in different positions and the contact and reaction with water vapor, and the defect that the uniformity and stability of product quality are difficult to guarantee.
[0008] Chinese patent 01131145.2 discloses "the method for preparing activated carbon from bamboo raw materials", in which there is no specific description about the equipment used, as far as the method used is concerned, there are both descriptions about the use of physical activation methods and descriptions about the use of chemical activation methods , but not very detailed
The consumption of raw materials for the production of one ton of activated carbon is: 3 to 5 tons by chemical method and 10 to 15 tons by physical method. Among them, when the physical method is used for activation, the carbon yield in the activation stage is less than 30%.

Method used

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  • Process for preparing bamboo-based activated carbon and dedicated device therefor
  • Process for preparing bamboo-based activated carbon and dedicated device therefor
  • Process for preparing bamboo-based activated carbon and dedicated device therefor

Examples

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preparation example Construction

[0050] The preparation method of bamboo activated carbon of the embodiment of the present invention may further comprise the steps:

[0051] a, crushing; the dried moso bamboo branches or branches are broken into fragments with a crusher, and the fragments with a particle size of 6 to 12mm are used for subsequent use;

[0052] b. Carbonization: Add broken bamboo pieces into the carbonization tube from the feed port on the top of the carbonization furnace, and the broken bamboo pieces will move down from the top of the carbonization tube along the carbonization tube under the action of gravity. The amount of steam added controls the carbonization temperature, and the carbonization time is controlled by discharging the material from the discharge pipe, so that the broken bamboo pieces are carbonized in the carbonization furnace to obtain carbonized materials. The carbonization temperature is 550-750°C, and the carbonization time is 1-4 hours;

[0053] c. Activation: Add the carb...

preparation example 1

[0057] a, the dried moso bamboo is broken into 6mm fragments with a crusher, and screened for subsequent use; b, the above-mentioned crushed material is carbonized in a multi-tube carbonization furnace, the carbonization temperature is 550 ° C, and the carbonization time is 4 hours; c, the above-mentioned The carbonization material is activated in the activation furnace, the activation temperature is 850°C, and the activation time is 72 hours. d. Soak the above-mentioned activation material in the pickling tank with a concentration of 3-5wt% hydrochloric acid solution for 1-3 hours, fully stir, and then Rinse with tap water for 3 to 5 times, then dehydrate, dry, screen and pack to obtain the finished activated carbon.

preparation example 2

[0059] a, the moso bamboo after drying is broken into 12mm fragments with a crusher, and screened for subsequent use; b, the above-mentioned crushed material is carbonized in a multi-tube carbonization furnace, the carbonization temperature is 750 ° C, and the carbonization time is 1 hour; c, the above-mentioned The carbonized material is activated in the activation furnace, the activation temperature is 950°C, and the activation time is 48 hours. d. The above-mentioned activation material is soaked in a pickling tank with a concentration of 3-5% hydrochloric acid solution for 1-3 hours, fully stirred, Then rinse with tap water for 3 to 5 times, then dehydrate, dry, screen and pack to obtain the finished activated carbon.

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Abstract

The invention discloses a preparing method and specific equipment of bamboo activated-carbon, which comprises the following steps: grinding; carbonizing continuously in the multi-pipe retort at 550-750 deg.c for 1-4 h; activating continuously in the retort at 800-950 deg.c for 48-72 h; pickling; bleaching; dehydrating; drying. The retort possesses stove base, furnace, several carbonizing pipes in the furnace vertically, feeder inlet on the top of retort, discharge device on the lower end, which is divided into preheating segment, carbonizing segment and cooling segment, wherein the retorting furnace contains furnace, heat-reserving chamber, chimney with furnace and heat-reserving chamber displaying left and right symmetrical structure; the furnace is separated into left and right half-furnaces by baffle; the heat-reserving chamber is divided into left and right two heat-reserving half-chamber correspondingly; the steam injecting pipe is set on the bottom of heat-reserving half-chamber; the vertical activating band is set in the furnace with several up-to-down carbonizing material channel and transverse gas flux to connect carbonizing material channel.

Description

technical field [0001] The invention relates to a preparation method of bamboo activated carbon and special equipment thereof, in particular to a method for preparing activated carbon by using bamboo branches and branches as raw materials and a carbonization furnace and an activation furnace used for realizing the method. Background technique [0002] Activated carbon is an excellent adsorbent with developed pore structure, large specific surface area and adsorption capacity. It is stable in nature, insoluble in water and organic solvents, resistant to acid and alkali, and easy to regenerate after use. There are many types of activated carbon, but the history of activated carbon manufacturing and application proves that compared with activated carbon produced from other raw materials, activated carbon produced from bamboo and wood materials has the advantages of large total pore volume, large specific surface area, large reactivity and less impurities. However, with the impr...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B31/08
Inventor 康锡军
Owner 浙江恒日炭业有限公司
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