The invention discloses a method for detecting tert-
butylamine residues in S-acetamidomethyl-L-
cysteine-L-
leucine tert-butyl ester, and mainly solves the problem that the existing method for detecting the tert-
butylamine residues in the S-acetamidomethyl-L-
cysteine-L-
leucine tert-butyl ester comprises the following steps: 1, preparing a sample, 2, carrying out
gas chromatography detection, and 3, detecting the tert-
butylamine residues in the S-acetamidomethyl-L-
cysteine-L-
leucine tert-butyl ester. According to the method, a
polyethylene glycol capillary
chromatographic column is mainly utilized, a gas chromatograph
hydrogen flame detector is combined, and the tert-butylamine residue in the S-acetamidomethyl-L-cysteine-L-leucine tert-butyl ester is calculated according to a
standard curve method.According to the method,
synchronous detection of a to-be-detected sample without interference is achieved, the
measurement precision is high, the method is simple, rapid and good in
repeatability, and the method is suitable for large-scale popularization and application of the tert-butylamine residue in the S-acetamidomethyl-L-cysteine-L-leucine tert-butyl ester. And a reliable and convenient detection means is provided for detecting the tert-butylamine residue in the S-acetamidomethyl-L-cysteine-L-leucine tert-butyl ester.