Method for extracting anthocyanin from lunar incense fructification
An anthocyanin and Cinnamomum cinnamon technology, applied in the field of extracting anthocyanins, can solve the problems of high price of plant natural pigments, low pigment substance content, long-time extraction and the like, and achieve the effects of high result rate, high purity and low raw material cost.
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Embodiment 1
[0018] 1. Harvesting of yin xiang fruit
[0019] Harvest black and mature Yinxiang fruits in late November or early December, rinse them with deionized water 1-2 times, wash off the dust on the surface of the fruits, remove sundries, rotten fruits, etc., and dry them for later use.
[0020] 2. Pretreatment of Cinnamomum yamba fruit
[0021] (1) Fresh fruit processing. Put the Yinxiang fruit into the pot, add water to submerge the Yinxiang fruit, quickly heat to boil, keep boiling for 10 minutes, take out the fruit, the peel cracks, quickly dissipate heat and cool down, after the fruit temperature drops to room temperature, stir to disintegrate the pulp tissue, The anthocyanins of fragrant fruit were only distributed in the tissues adjacent to the pericarp, and the pulp was separated from the core, but the structure of the core shell was well preserved.
[0022] (2) Dried fruit processing. The dried fruit of Yinxiang is soaked in deionized water with a pH value of 4 for 10 t...
Embodiment 2
[0036] Put the washed yin xiang fruit into the container, add water to submerge, heat and keep boiling for 60 minutes, take out the yin yang fruit, cool down to room temperature, stir the yin yang fruit to separate the pulp from the core; add 1 kg yin yang fruit pulp and fruit core In 1 liter of 60% ethanol aqueous solution or methanol aqueous solution, use acetic acid aqueous solution or sulfuric acid aqueous solution to adjust the pH value of the mixed solution to 5, soak at 50°C for 15 minutes, stir, filter, and collect the filtrate; Recover the alcohol solvent by distillation under reduced pressure at 0.09MPa, reduce the alcohol concentration of the filtrate to 9.5%, take the clear liquid after standing for 4 hours, and obtain the anthocyanin extract of Cinnamomum burmanii; use DA201, DM301, DS401 or DM-18 macroporous adsorption resin absorbs and separates anthocyanins from Cinnamomum burmanii, then elutes them with 30% ethanol aqueous solution or methanol aqueous solution,...
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