Functional rubber strengthening agent and preparation method thereof
A rubber reinforcing agent and a functional technology, applied in the field of functional additives and their preparation, can solve the problems of difficult control of conditions and low grafting rate, and achieve low hysteresis loss, high grafting rate and low heat generation. Effect
Inactive Publication Date: 2010-11-24
SHENYANG INSTITUTE OF CHEMICAL TECHNOLOGY
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Problems solved by technology
Considering the structure of starch and rubber, most of them use acids or acid anhydrides containing c=c double bonds to graft and modify starch, but the starch esters prepared by this method often have a very low grafting rate and the conditions are difficult to control
Method used
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Abstract
Provided is a functionality rubber strengthening agent and a relative preparation method, which relates to a chemical industry auxiliary agent and a preparation method thereof. The preparation method comprises a, under the condition of mechanical agitation, adding starch and initiating agent in a N, N-dimethylformamide solution whose temperature is 70-100DEG C to gelatinize for 0.5-2h, b, under the condition of mechanical agitation, adding hydroxyl protecting agent component A and protonic acid component B in the reactive solution of the first step, and reacting for 0.5-2h under the temperature of 70-100DEG C to prepare starch derivative via scouring, suction, drying and breaking, adding coupling agent to prepare the functionality rubber strengthening agent. The strengthening agent is simple in manufacturing technique, low in cost and comparatively high in environment-friendly extent, which is widely applied in various types of tires and other rubber products.
Description
A kind of functional rubber reinforcing agent and preparation method thereof technical field The invention relates to a chemical auxiliary agent and a preparation method thereof, in particular to a functional auxiliary agent used for rubber reinforcement, improving the elasticity of vulcanized rubber, reducing heat generation and hysteresis loss, and a preparation method thereof. Background technique Modified starch is a substance called "engineered biopolymer filler", which is obtained from ordinary starch through various modifications. In recent years, research on starch denaturation at home and abroad has progressed rapidly, and its products are widely used in textiles, food, medicine, petrochemicals, papermaking and other fields. However, starch is rarely used in rubber. Using starch as a reinforcing agent for rubber can obtain new rubber composite materials with low heat generation, high elasticity, and low hysteresis. Due to the limitations of the structure of star...
Claims
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Patent Type & Authority Patents(China)
IPC IPC(8): C08K5/10C08L3/08C08L21/00C08K5/54
Inventor 方庆红梁悦
Owner SHENYANG INSTITUTE OF CHEMICAL TECHNOLOGY
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