Chemical mechanical grinding fluid and chemical mechanical planarization method
A technology of chemical machinery and grinding slurry, which is applied in the direction of chemical instruments and methods, and other chemical processes, can solve unspoken problems such as chemical mechanical grinding, achieve the best production efficiency and commercial profit, improve grinding efficiency, and simple configuration.
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Embodiment 1-4
[0065] [Example 1-4] Preparation of Chemical Mechanical Polishing Slurry
[0066] Mix 300ml of sodium water glass with 2700ml of deionized water to form an aqueous solution of sodium silicate, pass it through a cation exchange resin column, and gradually A KOH aqueous solution with a concentration of 5wt% was added until the pH value of the sodium silicate aqueous solution was greater than 10, so as to carry out the polycondensation reaction of silicic acid. Then cool to 40° C., add 300 ml of a 10 wt % sodium aluminate aqueous solution, let it stand for 40 minutes to react, and then pass through the cation exchange resin column again to obtain a silica sol A with a clear appearance.
[0067] This silica sol A comprises several silicon dioxide grinding particles and aqueous medium which are modified by sodium aluminate and includes potassium, and the grinding particles are passed through a nanometer particle size analyzer (by De Rui Ke (TREKINTAL) Manufactured by the company, ...
Embodiment 2 and comparative example 2
[0117] After polishing the surface of the patterned wafer with the polishing slurry of Example 2, the contours of the components everywhere are slightly black, so the barrier layer (TaN) of the polished patterned wafer has been slightly eroded, avoiding some TaN barrier layer damage occurs.
[0118] Looking at the surface of the patterned wafer polished with the polishing slurry of Comparative Example 2, it is found that the contours of the components everywhere have turned black, which shows that the polishing slurry of Comparative Example 2 cannot prevent the patterned wafer from forming a tantalum nitride barrier layer at all. damage; therefore, compared with Comparative Example 2, the polishing slurry in Example 2 can prevent the barrier layer of the patterned wafer from being over-polished.
[0119] See also the efficacy data of each of the polishing slurries of Example 2 and Comparative Example 2 shown in Table 1. It is obvious that the polishing rate of copper (Example ...
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