Polymeric compositions containing nanotubes
A technology of polymers and compositions, applied in the direction of carbon nanotubes, single-walled carbon nanotubes, multi-walled carbon nanotubes, etc., can solve the problems of unsatisfactory practical applications, decreased mechanical strength and impact strength, and difficulty in obtaining sheets with satisfactory properties. Materials and other issues
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[0133] The compounding equipment was a high shear internal mixer Haake Rheocord 90 equipped with a mixing chamber with two counter-rotating Brabender-shaped blades. For each compound, the following method was used. The granular polymer is first introduced into the mixing chamber. Carbon black (Vulcan XC-500 carbon black) or thin thick multi-walled carbon nanotubes (MWNTs) are introduced into the mixing chamber.
[0134] At the end of the mixing cycle (1 minute at 40RPM / 40RPM to 200RPM in 3 minutes / 2 minutes at 200RPM), the compound was removed from the mixer and passed between two Mylar sheets on a hydraulic press Press down and flatten. The material was then cut into small pieces for a second mixing cycle to ensure good filler dispersion and a uniform compound.
[0135] Several compounds were prepared at different loadings (wt%) in EEA LE5861 obtained from Borealis with a nominal MFI of 6 g / 10 min at 190°C / 2.16 kg:
[0136] Carbon black: 35-30-25-20-17.5-15-12.5-10%
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