Catalyst layers having thin film mesh catalyst (TFMC) and fuel cell electrode assembly
A fuel cell electrode, fuel cell technology, used in fuel cell parts, fuel cells, battery electrodes, etc.
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example 1
[0092] Several mesh substrates were obtained made of copper and nickel, with platinum deposited on both sides of the substrates by means of sputtering. The thickness of the platinum deposit was controlled to provide a measure of catalyst loading. The nickel screen was provided with 750 lines per inch in the X and Y directions. A 0.00099" area of mesh openings with 55% porosity has a wire diameter of 0.00034", or a 0.025146 square millimeter area of mesh openings with 55% porosity has a diameter of 0.008636 millimeters. Deposit a 15 nm thick layer of platinum on the mesh using the sputtering technique. This is interpreted as per square centimeter (mg / cm 2 ) about 0.032 mg loading, which is much lower than that on commercially available MEA. TFMC thus prepared in Figure 4 is shown together with the GDL used in this example. Figure 4 Illustratively shown is a thin film catalyst with nickel base (TFMC) and 15 nm of platinum deposition with GDL.
[0093] Figure 6A to ...
example 2
[0098] Potential cycling prior to cyclic voltammetry (CV) was performed to test TFMC durability. The experiments were done in a 3-cell setup with 1 molar sulfuric acid. The CV was adjusted to sweep from -0.12V to 0.8V against a silver / silver chloride reference electrode. Potential cycling was processed as a square wave with an oscillating potential from 0.95V to 0.15V. Values from the CV procedure before and after 1800 cycles are depicted in FIG. 5 . Figure 5 depicts ADT for conventional GDE (a) and TFMC (b).
[0099] As demonstrated in Figure 5, the CV for conventional GDE changed significantly after 1000 minutes of the cycle, while the CV for TFMC showed very little change before or after cycling. Compared with conventional GDE, the exposed area of TFMC is very small, and as a result, the current in TFMC is relatively low.
[0100] Because it may be very expensive or impractical to have a single crystal of (111) on the entire surface of a mesh matrix carrier, an alte...
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