Production method of glucolactone
A technology of gluconolactone and a production method, which is applied in the production field of gluconolactone, can solve the problems of serious pollution, high resin consumption and high energy consumption, and achieves the effects of high concentration ratio, improved quality and low energy consumption
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[0042] Describe in detail below in conjunction with accompanying drawing and implementation example:
[0043] First filter the fermentation liquid containing sodium gluconate through a ceramic membrane, and then pass the continuous fluid separation device for continuous ion exchange to convert the sodium gluconate into gluconic acid solution, and then concentrate the gluconic acid solution through reverse osmosis to obtain gluconic acid concentrate. Add gluconolactone seed crystals to generate gluconolactone crystals in the concentrated solution (see figure 1 ). The specific operation process is as follows:
[0044] 1. Ceramic membrane filtration
[0045] The feed liquid used is gluconic acid fermentation liquid, the pore size of the ceramic membrane is 50nm, the temperature is 30°C, and the pressure is 0.3Mpa. A total of 3 batches of experiments have been carried out. The specific results are shown in Table 1:
[0046] the batch
when filtering
Room / h ...
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