Production method of glucolactone

A technology of gluconolactone and a production method, which is applied in the production field of gluconolactone, can solve the problems of serious pollution, high resin consumption and high energy consumption, and achieves the effects of high concentration ratio, improved quality and low energy consumption

Active Publication Date: 2010-03-17
厦门世达膜环保技术有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This new type of manufacturing technique uses special materials that help protect our environment from harmful chemicals while producing better products at lower costs compared to existing methods like conventional processes such as fermentation. It also allows us to produce various types of compounds without generating excessive amounts of residue. Additionally, there're no significant changes made during processing when changing between liquids. Overall, these technical improvements make them easier and cheaper to operate over longer periods of time.

Problems solved by technology

Technologies described involve producing glutocyanide from sugar sources like corn syrup. Current processes require expensive chemical reagents and complicated purifications techniques, resulting in poor yields and increased costs associated therewith.

Method used

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  • Production method of glucolactone
  • Production method of glucolactone
  • Production method of glucolactone

Examples

Experimental program
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Embodiment Construction

[0042] Describe in detail below in conjunction with accompanying drawing and implementation example:

[0043] First filter the fermentation liquid containing sodium gluconate through a ceramic membrane, and then pass the continuous fluid separation device for continuous ion exchange to convert the sodium gluconate into gluconic acid solution, and then concentrate the gluconic acid solution through reverse osmosis to obtain gluconic acid concentrate. Add gluconolactone seed crystals to generate gluconolactone crystals in the concentrated solution (see figure 1 ). The specific operation process is as follows:

[0044] 1. Ceramic membrane filtration

[0045] The feed liquid used is gluconic acid fermentation liquid, the pore size of the ceramic membrane is 50nm, the temperature is 30°C, and the pressure is 0.3Mpa. A total of 3 batches of experiments have been carried out. The specific results are shown in Table 1:

[0046] the batch

when filtering

Room / h ...

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Abstract

The invention discloses a production method of glucolactone, comprising the following steps: 1. ceramic membrane filtration and impurity removal: fermentation liquid is filtered by ceramic membrane filtration equipment to obtain sodium gluconate dialysate; 2. continuous fluid separation and conversion: the sodium gluconate dialysate enters into a continuous fluid separation device to carry out continuous ion exchange, so as to lead the sodium gluconate to be converted into sodium gluconate solution; 3. antiosmosis concentration: gluconic acid solution flown out from the continuous fluid separation device is contracted by an antiosmosis system to obtain gluconic acid concentrated solution; 4. crystallization: glucolactone inoculating crystal is added in the gluconic acid concentrated solution, so as to obtain the glucolactone. The method utilizes the ceramic membrane filtration to replace filter-bag filtration in the traditional process, adopts continuous fluid separation device to replace fixed bed ion exchange and uses fixed bed ion exchange to concentrate the gluconic acid, so as to improve the production yield of the glucolactone and reduce the production cost; the production method has the characteristics of energy saving and environmental protection.

Description

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Claims

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Application Information

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Owner 厦门世达膜环保技术有限公司
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