Grassleaf sweetflag rhizome extract, preparation method and application thereof
A technology of calamus calamus and its extract, which is applied in the field of extracts of calamus calamus and its preparation, can solve the problems of mutagenesis and carcinogenicity, and achieve the effects of high safety, low content, and improvement of learning and memory ability
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Example Embodiment
[0034] Example 1 Preparation of Acorus calamus extract SCP-B
[0035] Take 200g of Shichangpu medicinal material, add 2L (2000g) of water to slightly boil (100°C) to extract twice, 1h / time, and filter the extract. Concentrate to 400ml, use D101 type macroporous adsorption resin column, the column volume is 200ml, the amount of macroporous adsorption resin is 1g Shichangpu raw medicinal material / ml resin, respectively use 800ml water, 1000ml 10% ethanol solution, 1000ml 20% ethanol solution, Elute with 1000ml 30% ethanol solution, collect 20% ethanol eluate and 30% ethanol eluate, combine, concentrate and dry to obtain 4.3944g.
Example Embodiment
[0036] Example 2 Preparation of SIPI-SCP of Acorus calamus
[0037] Dissolve the Acorus calamus extract SCPB prepared in Example 1 in the upper phase (solvent system is chloroform-methanol-water=40%:40%:20%, volume percentage), the mobile phase is the lower phase, and the rotation speed is 800 rpm; The temperature is 25°C; the flow rate is 2.0ml / min, the peak after 350min is collected, concentrated and dried.
Example Embodiment
[0038] Example 3 Preparation of Acorus calamus extract SCP-B
[0039] Take 200g of Shichangpu medicinal material, add 1.6L (1600g) water, extract 3 times at 90°C, 15 minutes / time, and filter the extract. Add methanol to the extraction solution to a volume percentage of 60% methanol in the solution, collect the precipitate, add 100ml of water to dissolve it, and load it on a D101 macroporous adsorption resin column with a column volume of 500ml. The amount of macroporous adsorption resin is 0.1g Acorus calamus / ml resin, respectively eluted with 1000ml water, 1000ml 5% ethanol solution, 1000ml 15% ethanol solution, 1000ml 35% ethanol solution, collect 15% and 35% ethanol eluate, combine, concentrate and dry to obtain.
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap