Method for extracting natural Chinese herbal medicinal flavor component and application of extractive thereof

A technology for natural Chinese herbal medicines and aroma components, applied in the field of phytochemistry, can solve the problems of long extraction process time, single plant raw material, loss of natural aroma, etc., and achieve the effects of shortening extraction time, lowering extraction temperature, and improving internal quality.

Active Publication Date: 2010-09-22
江西省华宝孔雀食品科技发展有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, there are also a small amount of Chinese herbal medicine extracts used for flavoring tobacco, but most of them are single plant raw materials, and traditional Chinese medicine extraction methods are used, but the disadvantages of this method are: (1) The extraction process takes a long time and the temperature is high, and it is easy to make parts Loss of natural aroma; (2) In addition to useful ingredients, the product also contains some impurity ingredients with poor solubility. While improving the quality of cigarettes in some aspects, it also brings negative effects in other aspects to varying degrees. certain restrictions

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] (1) Raw material compounding: by weight, take 10 parts of honeysuckle, 23 parts of gardenia, 38 parts of medlar, 14 parts of bellflower and 11 parts of reed rhizome and mix to obtain raw materials;

[0025] (2) Ultrasonic treatment for the first time: In an ultrasonic extraction tank with a stirring and water bath heating device, add raw materials and deionized water, and perform the first ultrasonic treatment after soaking at 30°C for 2 hours; The ultrasonic temperature during ultrasonic treatment is 40°C, and the ultrasonic time is 50 minutes; the mass ratio of the raw material to deionized water is 1:11;

[0026] (3) collect the liquid obtained after the first ultrasonic treatment;

[0027] (4) Add deionized water of 8.5 times of raw material weight to the solid residue obtained after the first ultrasonic treatment, and carry out the second ultrasonic treatment; the ultrasonic temperature of the second ultrasonic treatment is 40 ° C, and the ultrasonic time is 40 mi...

Embodiment 2

[0035] (1) Compounding of raw materials: in parts by weight, 11 parts of honeysuckle, 25 parts of gardenia, 40 parts of wolfberry, 15 parts of bellflower and 12 parts of reed rhizome are mixed to obtain raw materials;

[0036] (2) Ultrasonic treatment for the first time: In an ultrasonic extraction tank with a stirring and water bath heating device, add raw materials and deionized water, and perform the first ultrasonic treatment after soaking at 35°C for 3 hours; The ultrasonic temperature during ultrasonic treatment is 50°C, and the ultrasonic time is 70 minutes; the mass ratio of the raw material to deionized water is 1:13.5;

[0037] (3) collect the liquid obtained after the first ultrasonic treatment;

[0038] (4) Add deionized water of 11 times the weight of the raw material to the solid residue obtained after the first ultrasonic treatment, and carry out the second ultrasonic treatment; the ultrasonic temperature of the second ultrasonic treatment is 50 ° C, and the ult...

Embodiment 3

[0046] (1) Compounding of raw materials: in parts by weight, 10.5 parts of honeysuckle, 24 parts of gardenia, 39 parts of Chinese wolfberry, 14.5 parts of bellflower and 11.5 parts of reed rhizome are mixed to obtain raw materials;

[0047](2) Ultrasonic treatment for the first time: In an ultrasonic extraction tank with a stirring and water bath heating device, add raw materials and deionized water, soak for 2.5 hours at 33°C and then perform the first ultrasonic treatment; The ultrasonic temperature during ultrasonic treatment is 45°C, and the ultrasonic time is 60 minutes; the mass ratio of the raw material to deionized water is 1:12;

[0048] (3) collect the liquid obtained after the first ultrasonic treatment;

[0049] (4) Add deionized water of 10 times the weight of the raw material to the solid residue obtained after the first ultrasonic treatment, and carry out the second ultrasonic treatment; the ultrasonic temperature of the second ultrasonic treatment is 45 ° C, an...

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Abstract

The invention relates to a method for extracting natural Chinese herbal medicinal flavor components. The method is characterized by comprising the following steps: (1) raw material formulation; (2) primary ultrasonic wave treatment, i.e. raw materials and deionized water are added into an ultrasonic wave extracting tank with stirring and water-bath heating devices, and the primary ultrasonic wave treatment is performed after dipping; (3) collection of fluid obtained after the primary ultrasonic wave treatment; (4) deionized water is added once again in solid residues obtained after the primary ultrasonic wave treatment for secondary ultrasonic wave treatment; (5) collection of fluide obtained after secondary ultrasonic wave treatment; (6) filtration; (7) primary concentration; (8) ethanol precipitation; and (9) secondary concentration. Application of the extractive comprises the following steps: weighing the extractive, dissolving the extractive in ethanol for forming; and spraying the extractive into cut fillers by adopting a laryngeal spray, and manufacturing the cut fillers to cigarettes. The invention has the advantages of shortening the extraction time and improving the extracting effect.

Description

technical field [0001] The invention relates to a method for extracting aroma components of natural Chinese herbal medicines and the application of the extract, which belongs to the technical field of phytochemistry. Background technique [0002] In tobacco products, the aroma and taste of tobacco are very important, and cigarette flavoring is one of the core technologies of the tobacco industry. Flavoring and flavoring can make up for the lack of cigarette leaf formula and eliminate The miscellaneous gas makes the aroma of the cigarette richer and more abundant, so that it has a unique style in smoking and smelling. As the harm-reducing effects of Chinese herbal medicines added to cigarettes are increasingly accepted by consumers, more and more tobacco scientific and technological workers are looking for flavors and fragrances for tobacco from Chinese herbal medicines. However, how to coordinate the aroma and taste of cigarettes with the aroma of Chinese herbal medicines h...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/00A24B15/26A24B3/12A61K36/899A61P11/14A61P11/10A61P11/06
Inventor 黄文华
Owner 江西省华宝孔雀食品科技发展有限公司
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