Quality control method for Chinese medicinal preparation Qinggong Shoutao pills
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A technology of traditional Chinese medicine preparations and detection methods, which is applied in measuring devices, instruments, scientific instruments and other directions to achieve the effect of improving quality control
Active Publication Date: 2012-02-29
津药达仁堂集团股份有限公司达仁堂制药厂
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[0004] The existing quality standards of Qinggong Shoutao Pills do not have specific identification methods for each component, but only describe it from the microstructure, which is not conducive to the qualitative and quantitative detection of the drug. It has brought great difficulties to the quality control of the drug. According to the search, there is currently no relevant patent on the quality control method of Qinggong Shoutao Pills. The existing patents mainly focus on the important formula and preparation method of Qinggong Shoutao Pills
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[0034] The following examples are used to further illustrate the present invention. The following examples are illustrative and not restrictive. The following examples cannot be used to limit the protection scope of the present invention.
[0035] The quality control method of traditional Chinese medicine preparation Qinggongshoutao Pills, the method steps are:
[0036] (1) Microscopic identification:
[0037] Observed under a microscope: the seed coat stone cells are light yellow to yellow, thick, wavy and curved, and the cell cavity contains brown material (medium berry). The thick-walled cells of the endothelium are yellowish-brown or reddish-brown, with thick walls, non-lignified, and the cell cavity contains siliceous blocks (Yizhi). Seed coat palisade cells are in slices, yellow-brown or light reddish-brown, polygonal-like, closely arranged, long columnar in lateral view, 60~145μm in length (sour date kernel). The undigested mesophyll tissue fragments contain many small clust...
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Abstract
The invention relates to a quality control method for a Chinese medicinal preparation Qinggong Shoutao pills, which comprises the following steps of: performing microscopical identification; and identifying whether the prescription of the Qinggong Shoutao pills comprises components such as Chinese angelica, medlar and dwarf lilyturf tuber or not by thin layer chromatography. On the basis of the primary standard, the microscopical identification method for the Qinggong Shoutao pills is modified, the descriptions of microscopical characteristics of ginseng and rehmannia root in the primary standard are deleted, the thin layer identification method for the Chinese angelica, the medlar and the dwarf lilyturf tuber is added, so that counterfeit medicines and inferior medicines can be more accurately inspected, the quality control of the medicines is improved, and the method has great significance for the modernization and internationalization of traditional Chinese medicines.
Description
technical field [0001] The invention belongs to the technical field of traditional Chinese medicines, and relates to a detection method of traditional Chinese medicines, in particular to a quality control method of Qinggong Shoutao Pills, a traditional Chinese medicine preparation. Background technique [0002] Qinggong Shoutao Pills are composed of donkey kidney, deer kidney, dog kidney, medlar, ginseng, asparagus, Ophiopogon japonicus, rehmannia glutinosa, angelica, puzzle (salt), silkworm excrement, wild jujube kernel (fried), distracting wood (fried ), its preparation method is: the above thirteen flavors are crushed into fine powder, sieved, mixed evenly, and 150-170 g of refined honey is added to each 100 g of powder to make a large honeyed pill. Yuan Qiangqiang is used for dizziness and fatigue caused by kidney deficiency and aging, memory loss, soreness of the waist and knees, tinnitus and deafness, vertigo and tearing, nocturia, and urination. [0003] Although th...
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