Antiseptic wear-resisting freezing adhesion-resisting one coat paint and preparation method thereof
An anti-corrosion, wear-resistant, anti-freezing and sticking technology, applied in anti-corrosion coatings, polyurea/polyurethane coatings, coatings, etc., can solve the problems of difficult anti-corrosion, wear-resistant, anti-icing, etc., and achieve good anti-corrosion effect.
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The preparation method of the anti-corrosion, wear-resistant, anti-freeze and adhesive bottom surface all-in-one coating provided by the present invention includes the following steps:
Preparation of component A: heat the amino-terminated polyether and fluorine-containing siloxane respectively to 100℃~120℃ for vacuum dehydration; mix isocyanate with anhydrous butyl acetate, heat up to 40℃~50℃ and start dripping after vacuum dehydration After the addition of the amino-terminated polyether and fluorine-containing siloxane, the mixture is heated to 80°C~90°C and kept for 1h~3h, the reaction is ended, the temperature is lowered to 40°C~50°C, and the product is obtained after discharge;
Preparation of component B: first mix and disperse dispersant, solvent and nano antifreeze adhesive material; then mix hindered aliphatic secondary amine, pigment filler, thixotropic agent and solvent, disperse, stir evenly, and grind to fineness ≤ 50μm; Finally, add the ultraviolet absorber nano ant...
Example Embodiment
Example 1:
1) Preparation of component A: 650Kg of amino-terminated polyether (Eastman) with a molecular weight of about 2000 and 50Kg of amino-terminated fluoropolysiloxane (molecular weight of 1800-2200) are heated to 120°C for vacuum dehydration;
Weigh 200Kg of isophorone diisocyanate (Bayer) and 160Kg of anhydrous butyl acetate, mix them evenly, heat up to 45°C and add dropwise the amino-terminated polyether and amino-terminated fluorine-containing polysiloxane after vacuum dehydration. After the addition, the temperature is raised to 80°C and kept for 2h, the reaction is ended, and the temperature is lowered to 45°C for discharging and packaging.
2) Preparation of component B:
The first step: Weigh 20kg of dispersant BYK163 (BYK company), 85kg of propylene glycol methyl ether acetate, and 30kg of nano zinc oxide whiskers to mix and use ultrasonic dispersion for 30min;
Step 2: Weigh sterically hindered aliphatic secondary amine polyaspartate resin (Bayer) 330kg, rutile ti...
Example Embodiment
Example 2:
1) Preparation of component A: 550Kg of amino-terminated polyether (Wuhan Shizishan Paint Factory) with a molecular weight of about 2000, and 80Kg of amino-terminated fluorinated polysiloxane (molecular weight of 1800-2200) are heated to 110°C for vacuum dehydration;
Weigh 270Kg of diphenylmethane diisocyanate and 100Kg of anhydrous butyl acetate, mix well, heat up to 40℃ and add dropwise the amino-terminated polyether and amino-terminated fluoropolysiloxane after vacuum dehydration. After the addition, the temperature is increased to 82 Heat for 1.5h at ℃, complete the reaction, and cool down to 40℃ for packaging.
2) Preparation of component B:
Step 1: Weigh 10kg of BYK163 dispersant (BYK company), 110kg of butyl acetate, and 70kg of nano-silicon carbide whiskers to mix and use ultrasonic dispersion for 30min;
Step 2: Weigh 350kg of hindered aliphatic secondary amine polyaspartate resin (Bayer), 90kg of rutile titanium dioxide (Dupon), 5kg of carbon black (Degussa...
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