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Electrode device and reaction atmosphere control system and method using electrode device

A technology for electrode devices and control systems, applied in the direction of electric heating devices, electrical components, feeding devices, etc., can solve the problems of high production costs, complicated atmosphere, and ineffective use of reaction atmosphere, so as to save consumption and increase production rate Effect

Active Publication Date: 2013-02-13
INST OF HIGH ENERGY PHYSICS CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] The object of the present invention is firstly to provide an electrode device capable of directing the reaction atmosphere into the arc discharge area, so as to solve the technical problems in the prior art that the atmosphere near the arc discharge area is complicated, the reaction atmosphere cannot be effectively utilized, and the production cost is high
[0009] The purpose of the present invention is also to provide a reaction atmosphere control system that can effectively control and adjust the reaction atmosphere in the arc discharge area, increase the output of carbon materials and save costs, so as to solve the problem of complex atmosphere and poor reaction atmosphere in the vicinity of the arc discharge area in the prior art. Technical problems of less than effective utilization and high production cost
[0010] The purpose of the present invention is also to provide a reaction atmosphere control method that can effectively control and adjust the reaction atmosphere in the arc discharge area, increase the output of carbon materials and save costs, so as to solve the problem of complex atmosphere near the arc discharge area and poor reaction atmosphere in the prior art. Technical problems of less than effective utilization and high production cost

Method used

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  • Electrode device and reaction atmosphere control system and method using electrode device
  • Electrode device and reaction atmosphere control system and method using electrode device
  • Electrode device and reaction atmosphere control system and method using electrode device

Examples

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no. 1 example

[0057] Such as figure 2 As shown, the electrode device of the first embodiment of the present invention mainly includes an electrode 20 , an outer cylinder 24 as a casing, and an insulating sheet 29 electrically insulating the electrode from the outer cylinder 24 . The gas path 22 is formed between the electrode 20 and the outer cylinder 24 .

[0058] Wherein, the electrode 20 as the cathode is arranged on the central axis position of the outer cylinder 24, and the electrode 20 is preferably a graphite rod, and the end of the electrode 20 is connected to the insulating sheet 29, and the front end of the electrode 20 stretches out of the outer cylinder 24 to be compatible with the outer cylinder 24. The anode is in contact with the counter electrode 31 for arc discharge. The axis position of the electrode 20 is connected with the connecting pipe 27, and the electrode device can be fixed to the synthesis furnace by means of the connecting pipe 27, and the cable for supplying p...

no. 2 example

[0063] The difference from the first embodiment is that if Figure 4 As shown, the outer cylinder 24 also includes an inner cylinder 28 made of insulating material, the inner cylinder 28 and the outer cylinder 24 together serve as the housing of the electrode device, and the electrodes 20 are arranged in the inner cylinder 28 with openings on both sides. The left side of the inner cylinder 28 is connected to the insulating sheet 29 , and an air passage 22 is formed between the outer wall of the inner cylinder 28 and the inner wall of the outer cylinder 24 . Other configurations such as electrodes 20, gas channel inlets 21, distribution holes 25, distribution chambers 26, connecting pipes 27 and insulating sheets 29 are the same as those in the first embodiment, and will not be repeated here.

[0064] The advantage of this embodiment is that the electrode 20 is further separated from the gas path 22 by setting the inner cylinder 28 made of electrically insulating material, so a...

no. 3 example

[0066] The difference from the previous two embodiments is that, if Figure 5 as shown, Figure 5 The cross-sectional view shown is located at Figure 4 Middle B-B, in this embodiment, the inner cylinder, outer cylinder and insulating sheet are integrally formed, all of which are insulating materials, and a cylinder with the same diameter as the distribution hole 25 is integrally formed between the inner cylinder 28 and the outer cylinder 24 Shape vent hole, with each vent hole as air path 22. image 3 and Figure 5 Among them, the number of distribution holes 25 is six.

[0067] In this embodiment, a plurality of individual air holes are used as the air passage 22 to make the air flow more stable and uniform.

[0068] Other components in the reaction atmosphere control system of the preferred embodiment of the present invention are introduced below.

[0069] Gas source 11 and gas source 12, such as gas storage devices such as gas cylinders: the stored gas can be an inert...

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Abstract

The invention discloses an electrode device and a reaction atmosphere control system and a method using the electrode device, which are used for fabricating carbon nano materials by an arc process, wherein the electrode device comprises an electrode, a shell and a gas circuit, wherein the electrode is arranged on the central axis of the shell, and one side of the shell is provided with an opening for causing the front end of the electrode to perform contact discharge with a counter electrode so as to form a discharge area; the shell and the electrode are electrically insulated through an insulator, the gas circuit surrounding the electrode is formed between the electrode and an external wall of the shell, and an outlet of the gas circuit is located at an outlet end of the shell, so that the gas in the gas circuit can be supplied to the discharge area. With the method and the system, the reaction atmosphere can be adjusted as required, so that dosage of inert gases and other reactant gases can be saved, and the productivity can be improved as well.

Description

technical field [0001] The invention relates to the technical field of synthesizing carbon materials by an arc method, in particular to an electrode device used for synthesizing carbon materials by an arc method, a reaction atmosphere control system and a reaction atmosphere control method using the electrode device. Background technique [0002] In the prior art, the arc discharge method is currently the most common method with the highest yield for preparing fullerenes. Usually, graphite rods are used as cathodes, graphite rods or metal composite graphite rods are used as anodes, and fullerenes and metallofullerenes are prepared at the same time as arc discharge. [0003] Arc discharge is usually carried out in a helium atmosphere, and the helium inlet is usually on the furnace body of the synthesis furnace (or electric arc furnace) for discharge synthesis. At present, most helium is imported from abroad, so the price is high, and the price of each bottle of helium is mor...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H05B7/06C01B31/02B01J4/00
Inventor 孙宝云董金泉赵宇亮
Owner INST OF HIGH ENERGY PHYSICS CHINESE ACAD OF SCI