Halogenated organic silicate ester flame-retardant plasticizer compound and preparation method thereof

A technology of flame retardant plasticizer and silicate, which is applied in the field of methyl silicate triester compound and its preparation, can solve the problems of high price and limitation of organosilicon products, and achieve high dual-element synergistic flame retardant efficiency, The effect of low cost and simple preparation method
CN102140112BActive Publication Date: 2013-02-27ENOVE PRECISION PLASTICS CATHETER

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
ENOVE PRECISION PLASTICS CATHETER
Publication Date
2013-02-27

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Abstract

The invention relates to a halogenated organic silicate ester flame-retardant plasticizer, namely a methyl silicate tri(2-chloroethyl) ester compound, and a preparation method thereof. The structure of the compound is shown as CH3Si(OCH2CH2Cl)3. The preparation method comprises the following steps of: introducing undersurface epoxy ethane with a certain molar ratio into methyl trichlorosilane under the cooling condition; reacting at the constant temperature for a certain period of time after the introduction; and removing excessive epoxy ethane and a small quantity of low-boiling-point substances by distilling to obtain colorless liquid methyl silicate tri(2-chloroethyl) ester. The methyl silicate tri(2-chloroethyl) ester has high flame retardance, high plasticity, a simple production process, small equipment investment and low cost, is environment-friendly and is easy for realizing industrial production.
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Description

technical field

[0001] The invention relates to a halogenated organosilicate flame retardant plasticizer compound and a preparation method thereof. Specifically relates to a methyl silicate tris (2-chloroethyl) ester compound and a preparation method thereof. Tris(2-chloroethyl)methylsilicate is a silicon-halogen-containing synergistic flame-retardant plasticizer, which is suitable for flame-retardant plasticizing additives of polyvinyl chloride, polyurethane, epoxy resin, unsaturated resin, etc. Background technique

[0002] With the wide application of polymer materials, because of its flammability, it often causes fires and poses a serious threat to people's lives and property, thus promoting the research of flame retardant technology and the rapid development of flame retardant plasticizer industry. Flame retardant plasticizer is a plastic processing aid with flame retardant function and plasticizing effect. It can overcome the problem of making polymer materials more f...

Claims

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