Composition of lucid ganoderma extract and tartary buckwheat extract, as well as application thereof
A technology of tartary buckwheat extract and ganoderma lucidum extract, applied in the field of extract composition
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Embodiment 1
[0051] Get 1.5kg of crushed Ganoderma lucidum, use 10 times, 8 times, 6 times the volume (i.e. 15 liters, 12 liters, 9 liters) of 95.0% ethanol to reflux extract 3 times, each time for 1h, after the ethanol is recovered from the extract, Load the sample on a diatomite column with a diatomite dosage of 2 kg, then elute with 6 times the column volume of ethyl acetate, collect the eluate, recover ethyl acetate, and obtain extract A; after extraction with the above-mentioned 95.0% ethanol Ganoderma lucidum dregs were decocted and extracted twice with 12 times and 10 times the volume of water, each time for 1 hour, the extract was concentrated to a relative density of 1.15, and then 95.0% ethanol was added until the alcohol content was 70%. After precipitation, filter and dry the filter cake to obtain extract B; combine extract A and extract B and mix uniformly to obtain 187.8 g of ganoderma lucidum extract;
[0052] Get 1.5kg of tartary buckwheat after crushing, use 10 times, 8 ti...
Embodiment 2
[0055] Get 1.5kg of crushed Ganoderma lucidum, extract by percolating with 85.0% ethanol of 25 times its volume (i.e. 37.5 liters), after the ethanol is recovered from the extract, the diatomite consumption is 1.8kg diatomite column, and then use Elute with 5 times column volume of ethyl acetate, collect the eluent, recover ethyl acetate, and obtain extract A; take the ganoderma lucidum dregs extracted with 85.0% ethanol, decoct with 15 times and 12 times the volume of water Boil and extract twice, 1 hour each time, concentrate the extract to a relative density of 1.18, then add 95.0% ethanol until the alcohol content is 65%, after complete precipitation, filter, take the filter cake and dry to obtain extract B; combined extraction Extract A and extract B were mixed uniformly to obtain 192.6 g of Ganoderma lucidum extract;
[0056] Get the tartary buckwheat 1.5kg after pulverizing, use the 85.0% ethanol percolation extraction of its 22 times amount volume (being 33 liters), af...
Embodiment 3
[0059] Get 1.5kg of crushed Ganoderma lucidum, use 8 times, 8 times, 6 times the volume (i.e. 12 liters, 12 liters, 9 liters) of 95.0% ethanol to reflux extract 3 times, each time for 1h, after the ethanol is recovered from the extract, Load the sample on a diatomite column with a diatomite dosage of 1.8 g, then elute with 4 times the column volume of ethyl acetate, collect the eluate, recover ethyl acetate, and obtain extract A; take the above-mentioned 95.0% ethanol for extraction The final ganoderma lucidum dregs were decocted and extracted twice with 10 times and 10 times the volume of water, each time for 1 hour, the extract was concentrated to a relative density of 1.13, and then 95.0% ethanol was added until the alcohol content was 70%. After complete precipitation, filter and dry the filter cake to obtain extract B; combine extract A and extract B and mix evenly to obtain 176.9 g of ganoderma lucidum extract;
[0060] Get 1.5g of tartary buckwheat after pulverization, ...
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