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Austenite grain size display method of wire rod for prestressed steel stranded wire

A prestressed steel strand, austenite grain technology, applied in particle size analysis, particle and sedimentation analysis, preparation of test samples, etc., can solve problems such as corrosion, shaking up and down, intermittent grain size, etc.

Inactive Publication Date: 2012-03-14
天津荣程联合钢铁集团有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the gradient quenching method, it is difficult to ensure that the part in the cooling liquid is always the same during the operation, and the quenching interface always shakes up and down due to hand shaking, so the final austenite grain size quenched is intermittent, which cannot truly reflect the actual condition of the steel. Heat treatment
The direct quenching method is relatively easy to operate, but due to the particularity of 82B steel, it is difficult to clearly display the austenite grain size by the general reagent display method
It is often a dark piece, and the boundary is either severely corroded or blurred, which makes it very difficult to evaluate the grain size, which in turn affects the results

Method used

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Experimental program
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Embodiment Construction

[0009] The present invention will be further described below.

[0010] first Preparation of the sample to be tested: Cut the 82B wire rod to be tested into 15cm-long strips by cold processing, heat it in a muffle furnace at 860±10°C for 45-75 minutes, and then clamp it with iron pliers for testing. The sample section is rapidly quenched and cooled in cooling water at room temperature; the quenched sample is tempered in a furnace at about 200 ° C for 1 hour, and the tempered wire rod section is ground, polished, cleaned and dried. is the sample to be tested;

[0011] Second, the preparation of the corrosive agent: add 6 grams of picric acid to 100 milliliters of distilled water and stir continuously, then add 5 drops of detergent and stir, and finally add 3 grams of copper sulfate and leave it for 12 hours;

[0012] Then corrode and polish: heat the above-mentioned etchant to 60°C, put it into the sample to be tested and corrode it for 1.5 minutes, take it out, rinse it wit...

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Abstract

The invention discloses a method capable of completely and clearly displaying the Austenite grain size of a wire rod for a prestressed steel stranded wire. The method is realized through the following steps of: preparing a test specimen to be tested: putting a 15cm-long wire rod in a muffle furnace at 860 DEG C plus or minus 10 DEG C for heating and then quenching and cooling the wire rod in cooling water at room temperature; tempering the wire rod for one hour in a furnace at approximately 200 DEG C; preparing corrosive agent: adding 6g of picric acid into 100ml of distilled water, continuously agitating, then adding five drops of cleanser essence, agitating, finally adding 3g of copper sulfate and placing for 12 hours; heating the corrosive agent to 60 DEG C, putting the test specimen to be tested in the corrosive agent to corrode the test specimen to be tested for 1.5 minutes, taking out the test specimen to be tested, repeating the corrosion and polishing steps for 3-5 times and finally conducting assessment through a comparison method against a standard map. The Austenite grain size testing method provided by the invention is a simple, convenient and high-efficiency 82B steel Austenite grain size testing method.

Description

technical field [0001] The invention relates to the field of metallographic analysis, in particular to a method for displaying the austenite grain size of wire rods for prestressed steel strands. Background technique [0002] At present, direct hardening method and gradient quenching method are used to detect the austenite grain size of wire rod (82B steel) for prestressed steel strand. In the gradient quenching method, it is difficult to ensure that the part in the cooling liquid is always the same during the operation, and the quenching interface always shakes up and down due to hand shaking, so the final austenite grain size quenched is intermittent, which cannot truly reflect the actual condition of the steel. Heat treatment condition. The direct quenching method is relatively easy to operate, but due to the particularity of 82B steel, it is difficult to clearly display the austenite grain size by the general reagent display method. It is often a dark piece, and the bo...

Claims

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Application Information

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IPC IPC(8): G01N15/02G01N1/28G01N1/32
Inventor 张洪卫
Owner 天津荣程联合钢铁集团有限公司
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