Epoxy resin matrix complex additive and preparation method thereof and modified polypropylene material
A polypropylene material and epoxy resin technology, which is applied in the field of compounding additives and preparation, can solve the problems of sticking equipment, mucus leakage, and sticky mucus, etc., and achieves the effects of high production efficiency, convenient operation and fast precipitation speed.
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[0013] A preparation method of epoxy resin-based composite auxiliary agent, comprising the following steps:
[0014] (1) According to the mass ratio, weigh the raw materials of the following components: nylon 6: epoxy resin: formic acid=1: 3.5-4.5: 3-6; see Table 1 for the specific formula.
[0015] Table 1 The mass ratio of each composition of epoxy resin-based composite additives
[0016] Example code
Nylon 6
epoxy resin
A
1
4
4
B
1
3.5
5
C
1
4.5
6
D
1
3
3
Remark
Grade: 1022B
Grade: E-44
industrial grade
[0017] (2) Add nylon 6 to formic acid to dissolve it, add epoxy resin to the formic acid solution in which nylon 6 is dissolved, and stir to obtain a uniform mixing system;
[0018] (3) Add water dropwise to the mixing system under stirring, epoxy resin and nylon 6 are precipitated together to form a white prec...
Embodiment 1
[0021] Mix the white powder of the prepared Example A formula with polypropylene at a ratio of 5% of the mass of the white powder to the polypropylene mass, and then add it to the twin-screw extruder at 210°C-220°C-230°C- Melt blending at an extrusion temperature of 225° C. (from the feed port to the discharge port) to obtain a modified polypropylene material. The modified polypropylene material and the pure polypropylene material were respectively tested according to the ASTM D790 standard for bending properties, ASTM D638 for tensile properties, and ASTM D256 for impact properties. The test results are shown in Table 2.
Embodiment 2
[0023] The white powder of the prepared Example A formula is mixed with polypropylene at a ratio of 10% of the mass of the white powder to the polypropylene mass, and then added to the twin-screw extruder at 210°C-220°C-230°C- Melt blending at an extrusion temperature of 225° C. (from the feed port to the discharge port) to obtain a modified polypropylene material. The modified polypropylene material and the pure polypropylene material were respectively tested according to the ASTM D790 standard for bending properties, ASTM D638 for tensile properties, and ASTM D256 for impact properties. The test results are shown in Table 2.
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