Method for preparing chromium-containing iron powder by direct reduction of calcium-free chromium slag
A technology of calcium-chromium-free slag and ferrochromium powder, applied in the direction of improving process efficiency, can solve the problems of high energy consumption, serious secondary pollution, low degree of resource utilization, etc., and achieves high recovery rate, reduced energy consumption, The effect of increasing the degree of resource utilization
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Embodiment 1
[0032] A method of preparing chromium-containing iron powder through direct reduction of calcium-free chromium slag in this embodiment, its process flow chart is as follows figure 1 As shown, the specific steps are as follows:
[0033] (1) Ingredients: mix calcium-chromium-free slag with reducing agent and flux, take 100 g calcium-chromium-free slag in the present embodiment, take 30 g anthracite coal powder as reducing agent, adopt X-ray fluorescence spectrometer and chemical analysis method to the above-mentioned The raw materials were analyzed. The physical and chemical indicators of calcium-free chromium slag and anthracite coal are shown in Table 1 and Table 2. X-ray diffraction analysis of calcium-free chromium slag shows that the minerals mainly include iron chromate, magnetite, forsterite, magnesium-iron Composition of olivine and silicate, from the chemical and phase analysis of calcium-free chromium slag, it can be seen that chromium slag mainly contains three eleme...
Embodiment 2
[0054] A kind of calcium-free chromium slag of the present embodiment prepares the method for chromium-containing iron powder through direct reduction, basically with embodiment 1, and the process parameter of its concrete steps is:
[0055] (1) Ingredients: Mix 100 g of calcium-free chromium slag with reducing agent and flux, wherein the flux is 9 g of alumina and 3 g of calcium fluoride, and the reducing agent is 30 g of anthracite coal powder. The quaternary alkalinity of the mixture is m(MgO+CaO) / m(SiO 2 +Al 2 o 3 )=0.9;
[0056] (2) Agglomeration: press the mixture in step (1) into cakes or pellets to obtain agglomerates;
[0057] (3) Reduction roasting: roast the blocks in step (2) in a reducing atmosphere, the reduction temperature is 1300 °C, and the time is 80 min;
[0058] (4) Crushing and fine grinding: crush the roasted block in step (3) and finely grind it to 80 meshes;
[0059] (5) Magnetic separation: The finely ground powder in step (4) was subjected to ma...
Embodiment 3
[0063] A kind of calcium-free chromium slag of the present embodiment prepares the method for chromium-containing iron powder through direct reduction, basically with embodiment 1, and the process parameter of its concrete steps is:
[0064] (1) Ingredients: Mix 100 g of calcium-free chromium slag with reducing agent and flux, wherein the flux is 1 g of alumina and 3 g of calcium fluoride, and the reducing agent is 30 g of anthracite coal powder. The quaternary alkalinity of the mixture is m(MgO+CaO) / m(SiO 2 +Al 2 o 3 )=1.3;
[0065] (2) Agglomeration: press the mixture in step (1) into cakes or pellets to obtain agglomerates;
[0066] (3) Reduction roasting: roast the blocks in step (2) in a reducing atmosphere, the reduction temperature is 1300 °C, and the time is 50 min;
[0067] (4) Crushing and fine grinding: crush the roasted block in step (3) and finely grind it to 120 mesh;
[0068] (5) Magnetic separation: The finely ground powder in step (4) was subjected to mag...
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