Adhesive composition for semiconductors, adhesive film, and semiconductor device
A technology of adhesives and compositions, applied in the field of adhesive compositions of semiconductors, can solve problems such as increasing void ratio, and achieve the effect of improving production efficiency
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Embodiment 1~10
[0140] Examples 1-10: Preparation of adhesive composition for semiconductor
[0141] As listed in Table 1, the solvent (I: cyclohexanone) was added to the acrylic resin, epoxy resin, curing agent, curing catalyst, filler and silane coupling agent so that the solid content in the solution was 40 wt%, and then the Mill kneading, thereby preparing an adhesive composition for semiconductors.
experiment example
[0160] Experimental Example: Evaluation of Physical Properties of Adhesive Films Prepared Using Adhesive Compositions in Examples and Comparative Examples
[0161] The physical properties of each of the adhesive films prepared using the adhesive compositions of Examples 1 to 10 and Comparative Examples 1 to 3 were evaluated by the following methods, and the results are provided in Table 5 and Table 6. The heat of cure was measured by differential scanning calorimetry (DSC), and the presence of voids after 1 cycle and molding was determined by ultrasonic tomography (SAT). After the reflow resistance test, cracks were observed with the naked eye and die shear strength was measured.
[0162] (1) Curing calorific value and exothermic peak height: The curing calorific value of the prepared adhesive composition was measured by DSC, the temperature rising rate was 10°C / min, and scanning was performed at 0-350°C.
[0163] The exothermic peak means the peak height of the exothermic pe...
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