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Mould material for detecting high-temperature fatigue performance and preparation method of mould material

A mold material and fatigue performance technology, which is applied in the high-temperature fatigue performance detection of plates and high-strength steel rods, can solve the problems of high cost of fine-grained materials, achieve the effects of preventing notch cracking, improving notch sensitivity, and increasing high-temperature strength

Inactive Publication Date: 2015-05-13
ANHUI UNIVERSITY OF TECHNOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The experimental temperature for high-temperature fatigue experiments is getting higher and higher, and the coarse-grained materials in the prior art cannot meet the requirements of the experimental conditions for the high-temperature strength and notch sensitivity of the test mold materials, while the fine-grained materials exist The problem of high cost, the present invention provides a mold material for high-temperature fatigue performance testing and its preparation method, which can be used as a low-cost material for testing molds for high-temperature fatigue performance of various alloys at 500-1000°C

Method used

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  • Mould material for detecting high-temperature fatigue performance and preparation method of mould material
  • Mould material for detecting high-temperature fatigue performance and preparation method of mould material

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Embodiment 1

[0034] A mold material used for high temperature fatigue performance testing, its composition elements and weight percentages are: Ni: 50%; Nb: 5%; Ti: 1.0%; C≤0.1%; the rest is Fe.

[0035] The preparation method of the mold material used for high temperature fatigue performance detection, the steps are:

[0036] A) Vacuum induction furnace smelting: the raw materials are subjected to vacuum induction furnace smelting according to the ratio of Ni: 50%; Nb: 5%; Ti: 1.0%; ;

[0037] B) Diffusion treatment of the steel ingot in a heating furnace at 1190°C for 5 hours, so that the composition of the steel ingot is uniform, and then air-cooled;

[0038] C) Heating the steel ingot to 1110°C, forging, air cooling after forging, the metallographic structure after forging is as follows figure 1 As stated, the detected grain size is 10 μm;

[0039] D) heat-preserve the forged steel ingot at 1100°C, heat it for 50 minutes, and then air-cool it. The grain size is 110 μm, as figure 2 S...

Embodiment 2

[0049] With embodiment 1, the difference is that the constituent elements and weight percent of the test material are: Ni: 40%; Nb: 6%; Ti: 0.8%; C≤0.1%; the rest is Fe; the steel ingot in step A) The radius is 149.7mm; in step B), the steel ingot is diffused in a heating furnace at 1200°C, and the holding time is 6.5h; in step C), the steel ingot is heated to 1120°C, and the grain size of the obtained material is d 0 is 15 μm; in step D), the forged steel ingot is subjected to heat preservation treatment at 1110° C. for 50 minutes, and the grain size d of the obtained material is 110 μm, and the relationship also satisfies the following relationship:

[0050] d 2.682 = d 0 2.682 + 4.733 × 10 18 t 1.313 exp [ - 295.406 / R ...

Embodiment 3

[0054] With embodiment 1, the difference is that the constituent elements and weight percent of the test material are: Ni: 60%; Nb: 4%; Ti: 1.2%; C≤0.1%; the rest is Fe; the steel ingot in step A) The radius is 153mm; in step B), the steel ingot is diffused in a heating furnace at 1180°C, and the holding time is 8.5h; in step C), the steel ingot is heated to 1100°C, and the grain size of the obtained material is d 0 is 12 μm; in step D), the forged steel ingot is subjected to heat preservation treatment at 1090 ° C for 50 minutes, and the grain size d of the obtained material is 110 μm, and the relationship also satisfies the following relationship:

[0055] d 2.682 = d 0 2.682 + 4.733 × 10 18 t 1.313 exp [ - 295.406 / R ...

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Abstract

The invention discloses a mould material for detecting high-temperature fatigue performance and a preparation method of the mould material, and belongs to the technical field of high-temperature fatigue performance detection of high-strength steel bars and steel plates. The mould material for detecting the high-temperature fatigue performance comprises the following elements by weight percentage: 40-60% of Ni, 4-6% of Nb, 0.8-1.2% of Ti, less than or equal to 0.1% of C, and the balance of Fe. The preparation method of the mould material comprises the steps of A) smelting in a vacuum induction furnace: smelting raw materials in the vacuum induction furnace at a ratio, and obtaining a steel ingot, B) diffusing the steel ingot in a heating furnace, C) heating and forging the steel ingot, and D) conducting thermal insulation on a forged billet. According to the mould material and the preparation method, a purpose of coarse-grain intensification above the equicohesive temperature is achieved by controlling a grain size; the cost is low; experimental temperature in a high-temperature fatigue experiment is increased; an application temperature range of the high-temperature fatigue experiment is expanded; and types of detected steel are increased.

Description

technical field [0001] The invention belongs to the technical field of high-temperature fatigue performance detection of high-strength steel rods and plates. Specifically, it relates to a kind of high-temperature fatigue performance that can be used in a relatively high temperature range (500-1000 ° C), and can be used for various The material of the test mold for testing the high-temperature fatigue performance of high-strength steel rods and plates and the preparation method of the material. Background technique [0002] Most engineering components are usually subject to alternating dynamic loads in use, that is, the magnitude or direction of the load changes with time. These alternating loads will cause fatigue damage to engineering materials. Even if the load value is lower than the yield strength of the material, repeated changes in the load will cause cyclic plastic deformation of the material, causing crack initiation, propagation, and final fracture. With the improv...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C19/03C22F1/10
Inventor 隋凤利徐丽霞朱国辉陈其伟
Owner ANHUI UNIVERSITY OF TECHNOLOGY