Preparation method of special flexible ceramic composite infiltration layer

A special ceramic and composite infiltration technology, applied in the direction of coating, metal material coating process, etc., can solve the problems of hardening technology and anti-corrosion technology single metal surface wear resistance or corrosion resistance, etc., to improve wear resistance and anti-corrosion. corrosive effect

Active Publication Date: 2013-08-14
SHANXI YITONG ENVIRONMENTAL ENERGY TECH GROUP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The present invention overcomes the problems existing in the prior art, and the technical problem to be solved is: general hardening technology and anti-corrosion technology can only improve the wear resistance or corrosion resistance of the metal surface

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] A preparation method of a tough special ceramic composite infiltrated layer is carried out according to the following steps:

[0035] a, cleaning the workpiece;

[0036] b. Preheating; put the cleaned workpiece into the salt bath furnace, heat it to 100°C and take it out;

[0037] c, infiltrating pottery; immerse the preheated workpiece in the prepared infiltrating pottery solution, and take it out after staying at a temperature of 520°C for 15 minutes;

[0038] Described osmosis pottery solution is prepared by weight with following raw materials:

[0039] TiO 3 : 15, Re—Mg: 15, ALF 3 : 16, KCl: 25, Al: 10, VCl 3 : 10, CaF 2 : 8, Na 2 B 4 o 2 : 20, SiC: 3, FeV: 5, W—Fe: 10, Mo—Fe: 10, V 4 o 5 : 5, Nb—Fe: 8, water: 50;

[0040] The above-mentioned raw materials are powders with a particle size of 300 mesh except water;

[0041] d, curing at low temperature; put the infiltrated workpiece into the passivation furnace, and take it out after staying at 160°C for ...

Embodiment 2

[0046] A preparation method of a tough special ceramic composite infiltrated layer is carried out according to the following steps:

[0047] a, cleaning the workpiece;

[0048] b. Preheating; put the cleaned workpiece into the salt bath furnace, heat it to 300°C and take it out;

[0049] c, infiltrating pottery; immerse the preheated workpiece in the prepared infiltrating pottery solution, and take it out after staying at 720°C for 180 minutes;

[0050] Described osmosis pottery solution is prepared by weight with following raw materials:

[0051] TiO 3 : 5, Re—Mg: 5, ALF 3 : 4, KCl: 10, Al: 2, VCl 3 : 3, CaF 2 : 3, Na 2 B 4 o 2 : 10, SiC: 1, FeV: 2, W—Fe: 5, Mo—Fe: 5, V 4 o 5 : 2, Nb—Fe: 2, water: 25;

[0052] The above-mentioned raw materials are powders with a particle size of 500 mesh except water;

[0053] d, curing at low temperature; put the infiltrated workpiece into a passivation furnace, and take it out after staying at a temperature of 300°C for 40 minut...

Embodiment 3

[0058] A preparation method of a tough special ceramic composite infiltrated layer is carried out according to the following steps:

[0059] a, cleaning the workpiece;

[0060] b. Preheating; put the cleaned workpiece into the salt bath furnace, heat it to 200°C and take it out;

[0061] c, infiltrating pottery; immerse the preheated workpiece in the prepared infiltrating pottery solution, and take it out after staying at a temperature of 620°C for 100 minutes;

[0062] Described osmosis pottery solution is prepared by weight with following raw materials:

[0063] TiO 3 : 10, Re—Mg: 10, ALF 3 : 10, KCl: 18, Al: 6, VCl 3 : 7, CaF 2 : 5, Na 2 B 4 o 2 : 15, SiC: 2, FeV: 3, W—Fe: 7, Mo—Fe: 8, V 4 o 5 : 3, Nb—Fe: 5, water: 30;

[0064] The above-mentioned raw materials are powders with a particle size of 350 mesh except water;

[0065] d, curing at low temperature; put the infiltrated workpiece into a passivation furnace, and take it out after staying at a temperature of ...

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PUM

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Abstract

The invention relates to a preparation method of a special flexible ceramic composite infiltration layer, which belongs to the technical field of a ceramic composite infiltration layer preparation method, and aims at solving the technical problem that a common hardening technology and a common anticorrosion technology can be only used for improving the abrasion resistance or the corrosion resistance of a metal surface. The preparation method provided by the invention is capable of simultaneously and greatly improving the abrasion resistance and the corrosion resistance of the metal surface. According to the technical scheme, the preparation method comprises the following steps of: a, washing a workpiece; b, preheating the workpiece; c, infiltrating the workpiece with ceramics; d, curing the workpiece at a low temperature; and e, drying the cured workpiece cleaned by clean water. After being processed by the method disclosed the invention, the workpiece has extremely high abrasion resistance, excellent corrosion resistance and good fatigue resistance, and only slightly deforms. The preparation method is suitable for processing the workpiece with high requirements on the abrasion resistance and the corrosion resistance and has a good effect.

Description

technical field [0001] The invention discloses a method for preparing a tough special ceramic composite infiltrated layer, belonging to the technical field of preparation methods for a ceramic composite infiltrated layer. Background technique [0002] The current common methods of preparing the infiltrated layer, such as ion sputtering, physical deposition, chemical plating, electroplating, spraying, melting, etc., all have the problem of the bonding strength between the molecules of the two substances. And usually the general hardening technology can only improve the wear resistance of the metal, and the anti-corrosion technology can only improve the corrosion resistance of the metal surface, and cannot greatly improve the wear resistance and corrosion resistance of the metal surface at the same time. Contents of the invention [0003] The invention overcomes the problems existing in the prior art, and the technical problem to be solved is: general hardening technology an...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C26/00
Inventor 张佑锋
Owner SHANXI YITONG ENVIRONMENTAL ENERGY TECH GROUP
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