Detection method for external traditional Chinese medicine preparation for treating haemorrhoids

The technology of a traditional Chinese medicine preparation and a detection method, which is applied in the field of medicine, can solve the problems affecting product production detection and medication safety, few detection indicators, and inability to effectively control the quality of compound Nepeta fumigation and washing preparations, and achieves a simple detection method and improved effective control. , the effect of high stability

Active Publication Date: 2013-09-25
RONGCHANG PHARM ZIBO CO LTD
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Clinically, it is mainly used for diseases such as external hemorrhoids, mixed hemorrhoids, prolapsed and incarcerated internal hemorrhoids, anal fissure, perianal abscess, or acute attack of anal fistula; Because the prescription contains toxic medicinal materials Aconitum aconitum and Aconitum aconitum, and there is no index limit for content determination, the quality detection method of the prior art cannot effectively control the quality of the compound Nepeta fumigation and washing preparation, which will affect the production of the product Testing and Medication Safety

Method used

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  • Detection method for external traditional Chinese medicine preparation for treating haemorrhoids
  • Detection method for external traditional Chinese medicine preparation for treating haemorrhoids
  • Detection method for external traditional Chinese medicine preparation for treating haemorrhoids

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Embodiment 1

[0052] The external Chinese medicinal preparation for treating hemorrhoids of the present invention is made from the following raw materials in parts by weight:

[0053]Nepeta 120g Fangfeng 120g Sperantos 300g

[0054] Sichuan Aconitum 90g Frog Grass 300g Grass Aconitum 90g

[0055] Sophora flavescens 120g.

[0056] The preparation method is as follows:

[0057] Firstly crush Nepeta, Aconitum Aconitum, and Aconitum Aconitum into fine powder, then decoct the rest of the raw materials with water for 2, 2, and 1 hours respectively, combine the decoctions, filter, concentrate the filtrate under reduced pressure, and dry , crushed into fine powder, and finally the two fine powders are combined and mixed, granulated and dried.

[0058] Identification of contents:

[0059] The specific steps of the identification method of Nepeta chinensis are as follows:

[0060] Take the sample and grind it finely, weigh 6g, add 30ml of acetone and sonicate for 30 minutes, filter, evaporate th...

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Abstract

The invention belongs to the technical field of medicines, and particularly relates to a detection method for an external traditional Chinese medicine preparation for treating haemorrhoids. The external traditional Chinese medicine preparation for treating haemorrhoids is prepared from the following raw materials in parts by weight: 105-135 parts of fineleaf schizonepeta herb, 105-135 parts of radix saposhnikoviae, 270-330 parts of garden balsam stem, 80-100 parts of radix aconiti, 270-330 parts of bothriospermum chinense, 80-100 parts of radix aconiti kusnezoffii and 105-135 parts of radix sophorae flavescentis. The detection method for the external traditional Chinese medicine preparation for treating haemorrhoids comprises identification of contents and measurement of component content, wherein the identification of contents is the identification of fineleaf schizonepeta herb, radix saposhnikoviae, monkshood and radix aconiti kusnezoffii by thin layer chromatography; and the measurement of component content is the measurement of the content of sophocarpidine and aconitum alkaloids by high performance liquid chromatography. The method provided by the invention is simple, convenient, quick and accurate, has good sensitivity and high stability, improves the effective control on the drug quality, and guarantees the quality.

Description

technical field [0001] The invention belongs to the technical field of medicines, and in particular relates to a detection method of an external Chinese medicinal preparation for treating hemorrhoids. Background technique [0002] Compound nepeta fumigation and washing preparation, as a traditional Chinese medicine preparation for external use in the treatment of hemorrhoids, has the functions of dispelling wind and dampness, reducing swelling and relieving pain. Clinically, it is mainly used for diseases such as external hemorrhoids, mixed hemorrhoids, prolapsed and incarcerated internal hemorrhoids, anal fissure, perianal abscess, or acute attack of anal fistula; Because the prescription contains toxic medicinal materials Aconitum aconitum and Aconitum aconitum, and there is no index limit for content determination, the quality detection method in the prior art cannot effectively control the quality of the compound Nepeta fumigation and washing preparation, which will affe...

Claims

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Application Information

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IPC IPC(8): A61K36/73A61P9/14G01N30/02G01N30/90
Inventor 郭桂秋翟勇王荔强高娇王园玲胡军
Owner RONGCHANG PHARM ZIBO CO LTD
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