Iron base soft magnetic powder for powder magnetic core, fabrication method for same, and powder magnetic core
A powder magnetic core and soft magnetic technology, which is applied to the iron-based soft magnetic powder for powder magnetic core and the manufacture of iron-based soft magnetic powder for the powder magnetic core and the field of powder magnetic core, which can solve the problems of high cost and achieve improved durability. Thermal properties, low iron loss, and high heat resistance
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[0023] The present inventors formed a powder compact of an iron-based soft magnetic powder base material on which a coating film composed of only phosphoric acid or a glassy insulating layer obtained from phosphoric acid described in Patent Document 1 was formed, and obtained a pressed powder. Powder shaped body (powder core). Furthermore, the present inventors measured the electrical resistivity (μΩ·m) of the powder compact by changing the temperature. As a result, in all cases, it was confirmed that the resistivity of the compact was lowered to about 10 μΩ·m by the treatment at 450° C. (under a nitrogen atmosphere, for 1 hour).
[0024] The inventors of the present invention studied the cause of the decrease in resistivity, and as a result, it is speculated that oxygen atoms derived from phosphoric acid contained in the phosphoric acid-based film diffused during heat treatment at a high temperature and bonded to Fe to form oxidation of Fe that functions as a semiconductor. ...
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