Insulating film-coated metal foil
A technology of metal foil and insulating film, applied in the direction of insulators, metal layered products, metal material coating technology, etc., can solve the problems of low flexibility and inappropriate silicon dioxide insulating film, etc., and achieve the effect of improving the yield
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no. 1 Embodiment approach ]
[0055] The first embodiment is a method for producing an insulating film-coated metal foil having an organic-inorganic hybrid material layer, wherein polydimethylsiloxane or the like having an average molecular weight Mw=900 to 10,000 and a compound having a compound selected from Mg, Ca, Metal alkoxides of one or more metals among Y, Al, Sn, Ti, Zr, Nb, Ta, and W are synthesized in an organic solvent to obtain a sol, and the sol is coated on the surface of a SUS foil to form a film.
[0056] (polydimethylsiloxane, etc.)
[0057] Polydimethylsiloxane, dimethyldialkoxysilane, dimethyldichlorosilane, and the like can be used. From the viewpoint of easiness of obtaining a flexible film, polydimethylsiloxane is preferably used.
[0058] Polydimethylsiloxane refers to a substance formed by bonding two methyl groups to Si and continuously bonding Si-O siloxane in a straight chain. The general formula X-[-Si(CH 3 ) 2 -O-] n -Si(CH 3 ) 2 -X means. Wherein, X is a reactive funct...
no. 2 Embodiment approach ]
[0106] The second embodiment is an insulating film-coated metal foil comprising at least a metal foil 10 and an organic-inorganic hybrid material layer 11 ( figure 1 ).
[0107] Concentration of Si at a depth of 1 / 4t from the surface of the layer along the thickness direction of the organic-inorganic hybrid material layer [Si] 1 / 4t Relative to the concentration of Si at a depth of 3 / 4t from the surface of the organic-inorganic hybrid material layer along the thickness direction of the layer [Si] 3 / 4t , has the following relation, [Si] 1 / 4t 3 / 4t , and the relative ratio of the above Si concentration, R Si =[Si] 3 / 4t -[Si] 1 / 4t / [Si] 3 / 4t The value of is 0.02 or more and 0.23 or less.
[0108] Furthermore, the concentration of Si at a depth of 1 / 2t from the surface of the layer along the thickness direction of the organic-inorganic hybrid material layer [Si] 1 / 2t , Concentration of metal element M with metalloxane containing metal elements other than Si [M]1 / 2t Ratio A 1...
Embodiment
[0136] (Coating Solution A)
[0137] Metal alkoxides are used as precursors of metalloxanes, and polydimethylsiloxanes are used as precursors of dimethylsiloxanes. A metal alkoxide made by mixing 8 moles of titanium tetraisopropoxide with ethyl 3-oxobutyrate as a chemical modifier in an amount of 16 moles which is twice the amount of titanium tetraisopropoxide substance. 2.5 moles of polydimethylsiloxane (terminal groups are silanols) having a mass average molecular weight of 3000 were added to the chemically modified titanium alkoxide. Add 1 mole of 1-butanol to the above mixture as a solvent to adjust the viscosity, and then add 5 moles of H 2O, prepare coating solution A.
[0138] (Coating solution B)
[0139] Metal alkoxides are used as precursors of metalloxanes, and polydimethylsiloxanes are used as precursors of dimethylsiloxanes. For the metal alkoxide, titanium tetraisopropoxide was 2 moles, and ethyl 3-oxobutyrate was mixed as a chemical modifier thereof in an a...
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