Method of producing substitute natural gas by methanation of synthesis gas
A technology to replace natural gas and gas methane, applied in the direction of gas fuel, petroleum industry, fuel, etc., can solve the problems of excess components, large amount of circulating gas, and high energy consumption of compressors, and achieve short reaction process, reduced circulating gas volume, and CO conversion rate-enhancing effect
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Embodiment 1
[0034] A certain 1.2 billion Nm 3 / year synthetic gas to replace natural gas plant (8000 operating hours per year), using figure 1 The high-temperature methanation and low-temperature methanation reaction zones are both two-stage, and the catalysts loaded therein are all Ni-based catalysts (where Al 2 o 3 Carrier 60%, Nickel 35%). The composition of raw syngas 1 is: (H 2 -CO 2 ) / (CO+CO 2 )=3.1, pressure 3.5MPa, feed rate 600,000 Nm 3 / h, divided into two parts, the ratio of the first-stage synthesis gas 2 and the second-stage synthesis gas 3 is 1:1.5, and the stream 4 after the first-stage synthesis gas 2 and the cycle gas 8 is mixed enters the first-stage high-temperature methanation reaction at a temperature of 300°C The methanation reaction occurs in the reactor 101, the volume ratio of the recycle gas 8 and the first-stage synthesis gas 2 is 2.4:1, the temperature of the reaction outlet stream 5 is 650°C, and after cooling by the outlet cooler 105 of the first-stage ...
Embodiment 2
[0038] A certain 1.2 billion Nm 3 / year synthetic gas to replace natural gas plant (8000 operating hours per year), usingfigure 1 process technology, the composition of raw syngas is: (H 2 -CO 2 ) / (CO+CO 2 ) = 3.2, the mixed stream 4 of the first-stage synthesis gas 2 and the recycle gas 8 enters the first-stage high-temperature methanation reactor 101 at a temperature of 320°C and a pressure of 4.5 MPa to undergo methanation reaction, the volume of the recycle gas 8 and the first-stage synthesis gas 2 The ratio is 2:1, the temperature of the reaction outlet stream 5 is 700°C, the inlet temperature of the secondary high-temperature methanation reactor 102 is 320°C, the outlet temperature is 700°C, the pressure is 4.2 MPa, and CO 2 The gas volume is 12000Nm 3 / h, the volume ratio of material 7 and material 8 is 1.53, the volume ratio of material 5 and material 3 is 1.65, the volume ratio of material 13 and material 10 is 0.055, and all the other conditions are the same as [e...
Embodiment 3
[0042] A certain 1.2 billion Nm 3 / year synthetic gas to replace natural gas plant (8000 operating hours per year), using figure 1 process technology, the composition of raw material synthesis gas 1 is: (H 2 -CO 2 ) / (CO+CO 2 ) = 3.1, pressure 5.0MPa, divided into two parts, the ratio of the first-stage synthesis gas 2 and the second-stage synthesis gas 3 is 1:1, the volume ratio of the recycle gas 8 and the first-stage synthesis gas 2 is 2:1, and the first-stage synthesis gas 2 The stream 4 mixed with the circulating gas 8 enters the first-stage high-temperature methanation reactor 101 at a temperature of 290°C to undergo a methanation reaction, and the temperature of the reaction outlet stream 5 is 640°C, and is cooled by the outlet cooler 105 of the first-stage high-temperature methanation reactor , the material 6 mixed with the second-stage synthesis gas 3 enters the secondary high-temperature methanation reactor 102 at 300°C, and the reaction outlet stream 7 has a tempe...
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