A kind of leaching repair method of molybdenum polluted soil
A technology of polluted soil and remediation method, applied in the direction of restoration of polluted soil, etc., to achieve the effect of maintaining productivity, easy operation and wide adaptability
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Embodiment 1
[0017] A kind of leaching method for remediating molybdenum-contaminated soil is:
[0018] 1. Take 5.00 g of a molybdenum-contaminated soil (total molybdenum content of the soil is 54.73 mg / kg) in a 50 ml centrifuge tube, add Na at a concentration of 0.10 mol / L 3 PO 4 Solution 25ml.
[0019] 2. Place the centrifuge tube in a parallel shaker at room temperature (25±3°C) at a shaking rate of 200 rpm for 1.5 hours.
[0020] 3. Place the shaken centrifuge tube in a centrifuge, centrifuge at a speed of 3000 rpm for 10 minutes, and discard the supernatant.
[0021] 4. Add 25 ml of eluent to the residual soil, shake the soil at the bottom of the centrifuge tube by hand, and then place the centrifuge tube in a parallel shaker. At room temperature (25±3°C), the shaking rate is 200 rpm, shake for 1.5 hours.
[0022] 5. Place the shaken centrifuge tube in a centrifuge, centrifuge at a rate of 3000 rpm for 10 minutes, and pour off the supernatant.
[0023] 6. Add 25 ml of eluent to...
Embodiment 2
[0027] A kind of leaching method for remediating molybdenum-contaminated soil is:
[0028] 1. Take 5.00 g of a molybdenum-contaminated soil (the total molybdenum content of the soil is 93.74 mg / kg) in a 50 ml centrifuge tube, add Na at a concentration of 0.10 mol / L 3 PO 4 Solution 25ml.
[0029] 2. Place the centrifuge tube in a parallel shaker at room temperature (25±3°C) at a shaking rate of 200 rpm for 1.5 hours.
[0030] 3. Place the shaken centrifuge tube in a centrifuge, centrifuge at a speed of 3000 rpm for 10 minutes, and discard the supernatant.
[0031] 4. Add 25 ml of eluent to the residual soil, shake the soil at the bottom of the centrifuge tube by hand, and then place the centrifuge tube in a parallel shaker. At room temperature (25±3°C), the shaking rate is 200 rpm, shake for 1.5 hours.
[0032] 5. Place the shaken centrifuge tube in a centrifuge, centrifuge at a rate of 3000 rpm for 10 minutes, and pour off the supernatant.
[0033] 6. Add 25 ml of eluen...
Embodiment 3
[0037] A kind of leaching method for remediating molybdenum-contaminated soil is:
[0038] 1. Take 5.00 g of a molybdenum-contaminated soil (total molybdenum content in the soil is 127.49 mg / kg) in a 50 ml centrifuge tube, add Na at a concentration of 0.10 mol / L 3 PO 4 Solution 25ml.
[0039] 2. Place the centrifuge tube in a parallel shaker at room temperature (25±3°C) at a shaking rate of 200 rpm for 1.5 hours.
[0040] 3. Place the shaken centrifuge tube in a centrifuge, centrifuge at a speed of 3000 rpm for 10 minutes, and discard the supernatant.
[0041] 4. Add 25 ml of eluent to the residual soil, shake the soil at the bottom of the centrifuge tube by hand, and then place the centrifuge tube in a parallel shaker. At room temperature (25±3°C), the shaking rate is 200 rpm, shake for 1.5 hours.
[0042] 5. Place the shaken centrifuge tube in a centrifuge, centrifuge at a rate of 3000 rpm for 10 minutes, and pour off the supernatant.
[0043] 6. Add 25 ml of eluent t...
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