Novel magnetic refrigerant materials
A magnetic refrigeration and magnetic heating technology, applied in the direction of magnetic materials, inorganic materials, heat exchange materials, etc.
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[0096] Three kinds of Ni having the atomic composition ratio specified in this specification were induction-melted under Ar atmosphere 50 mn 50-x In x-y Si y alloy. Two ingots cast in two batches have the same Ni 50 mn 35 In 14 Si composition, while the third ingot has Ni 51 mn 33.4 In 15.6 Element. Samples processed from as-cast ingots were subsequently heat-treated in two steps in a flowing Ar furnace.
[0097] In the first step, the sample is annealed at a temperature of about 800°C to about 900°C for 4 hours to 24 hours. After the first annealing step, the samples were quenched to room temperature (about 20° C.) in a water bath. In a second step, the sample was annealed at a temperature of about 500°C to about 700°C for 48 hours to 72 hours, and then quenched again in a water bath to room temperature.
[0098] Martensite and austenite were determined based on magnetization and temperature data collected with respect to an applied magnetic field of 10 mTesla usi...
example 1
[0100] Ni at various temperatures and durations 50 mn 35 In 14 Si alloy (Ni 50 mn 35 In 14 Si-sample PV-9582) was heat treated. The martensitic transformation temperature, or MPTT, of this as-cast billet was 261K. By changing the heat treatment parameters, the transformation temperature of the alloy can be adjusted between about 261K and about 268.5K, as shown in Table 1 and Figure 4 shown.
[0101] Table 1.Ni 50 mn 35 In 14 Si alloy (Ni 50 mn 35 In 14 Martensitic transformation temperature and heat treatment parameters in Si-batch 1).
[0102]
example 2
[0104] Ni at various temperatures and durations 50 mn 35 In 14 Si alloy (Ni 50 mn 35 In 14 Si-sample SA01) was heat treated. The martensitic transformation temperature of this as-cast ingot is 265K. By changing the heat treatment parameters, the transformation temperature of the alloy can be adjusted between about 265K and about 271.5K, as shown in Table 2 and Figure 5 shown.
[0105] Table 2.Ni 50 mn 35 In 14 Si alloy (Ni 50 mn 35 In 14 Martensitic transformation temperature and heat treatment parameters in Si-batch 2).
[0106]
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