Preparation of wc-ni micro parts, cutting tools and their preparation methods based on multi-physics field activation sintering
A technology of micro-parts and activated sintering, applied in other manufacturing equipment/tools, mechanical equipment, engine components, etc., can solve the problems of low product purity, serious product pollution, long sintering time, etc., and achieve simplified process flow and mechanical properties Excellent, short holding time effect
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Embodiment 1
[0032] The sample used in the experiment is a Φ4*4mm cylinder and the theoretical density of the corresponding powder is used to calculate the powder mass. WC powder and Ni powder are mixed by wet grinding method according to the weight ratio of 94:6. After weighing, put the mixed powder into the mold chuck and fix it. Under the condition of vacuum degree ≤ 0.01Pa, adjust the heating rate to 50°C / s, and simultaneously apply a force of 85MPa to both ends of the mold. When the temperature reaches 300°C, keep it warm for 80s, then adjust the heating rate to 60°C / s, heat it to 1150°C and keep it warm for 10 minutes, the powder is formed in the mold and sintered, and finally cooled to room temperature at a cooling rate of 15°C / s , turn off the power and take out the parts. The relative density of the sample is 98.3%, the fracture toughness Kic is 10MPa·m1 / 2, and the product has no obvious Ni pool.
Embodiment 2
[0034] The sample used in the experiment is a Φ4*4mm cylinder and the theoretical density of the corresponding powder is used to calculate the powder mass. WC powder and Ni powder are mixed by wet grinding method according to the weight ratio of 90:10. After weighing, put the mixed powder into the mold chuck and fix it. Under the condition of vacuum degree ≤ 0.01Pa, adjust the heating rate to 25°C / s, and simultaneously apply a force of 65MPa to both ends of the mold. When the temperature reaches 180°C, keep it warm for 50s, then adjust the heating rate to 50°C / s, when heated to 1350°C, keep it warm for 8 minutes, the powder is formed in the mold and sintered, and finally cooled to room temperature at a cooling rate of 10°C / s , turn off the power and take out the parts. The relative density of the sample is 99.3%, and the HV30 is 2121kgf / mm 2 , the fracture toughness Kic is 10.1MPa m1 / 2, and the product has no obvious Ni pool.
Embodiment 3
[0036] The sample used in the experiment is a Φ4*4mm cylinder and the theoretical density of the corresponding powder is used to calculate the powder mass. Mix WC powder and Ni powder by wet grinding method according to the weight ratio of 88:12. After weighing, put the mixed powder into the mold chuck and fix it. Under the condition of vacuum degree ≤ 0.01Pa, adjust the heating rate to 40°C / s, and simultaneously apply a force of 95MPa to both ends of the mold. When the temperature reaches 270°C, keep it warm for 100s, and then adjust the heating rate to 65°C / s. After heating to 1400°C, it is sintered 13 times in the range of 1400°C-800°C. The powder is formed in the mold and sintered, and finally Cool to room temperature at a cooling rate of 10°C / s, then turn off the power and take out the parts. The relative density of the sample is 99.5%, and the HV30 is 2096kgf / mm 2 , the fracture toughness Kic is 12.1MPa m1 / 2, and the product has no obvious Ni pool.
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