Detection method of medicinal preparation for treating arthralgia
A detection method and technology for pharmaceutical preparations, which are applied in measurement devices, color/spectral property measurement, instruments, etc., can solve the problem that the material basic research of Jingulian Capsule is not perfect, the active ingredients have not been clarified, and the accuracy of quality standard identification cannot be guaranteed. issues of sex
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Embodiment 1
[0158] Embodiment 1: Preparation of Jingulian capsule for the treatment of joint swelling and pain
[0159] Prescription: Touguxiang 343g, Chinese peach leaves 400g, Daxueteng 370g, star anise maple 50g, golden iron lock 50g, starch 125g;
[0160] Preparation method: the above five flavors of medicinal materials, Jin Tie Suo, add water and decoct for 3 hours, filter, the filtrate is set aside, the dregs of the medicine are dried and crushed into fine powder, and set aside; the remaining four flavors such as Touguxiang are decocted with water for three times, each time for 2 hours, combined Decoction, filter, combine the above filtrates, concentrate to 60°C and measure the clear paste with a relative density of 1.25-1.28; add the above-mentioned fine powder and starch, mix well, dry, crush, sieve, pack into capsules, and make 1000 capsules .
Embodiment 2
[0161] Embodiment 2: the detection method of Jingulian capsule for the treatment of joint swelling and pain consists of the following contents:
[0162] Properties: This product is a capsule, the content is yellow-brown to reddish-brown powder; slight gas, slightly bitter taste;
[0163] Identification: (1) Identification of Tou Guxiang: Take 3g of the content of this product, add 30ml of methanol, heat and reflux for 30 minutes, filter, and concentrate the filtrate to 0.5ml, as the test solution; Prepare the reference medicinal material solution in the same way; according to the Chinese Pharmacopoeia 2010 edition, appendix VIB thin-layer chromatography test, draw 5 μl of each of the above two solutions, and spot them on the same silica gel G thin-layer plate with sodium carboxymethyl cellulose as the binder. Above, use chloroform: acetone = 9:1 as developer, develop, take out, dry in the air, fumigate with concentrated ammonia test solution for about 5 minutes, and observe un...
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