Enhanced slag formation for copper-containing gas generants
A gas generating agent and slag-making technology, which can be used in the production of compressed gas, attack equipment, non-explosive/non-thermal agent components, etc., and can solve problems such as adverse effects on system efficiency
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example 1
[0060] Experiments were conducted to determine the effect of aluminum hydroxide particle size on slagging in a typical gas generant formulation. Comparative Example 1 was conventional smaller sized aluminum hydroxide particles, while Example 2 was prepared according to certain aspects of the present teachings. Table 2 shows the components and properties of the gas generants of Comparative Example 1 and Example 2.
[0061]
[0062]
[0063] Table 2
[0064] The above two formulations were prepared separately and pressed into 0.5" diameter x 0.43" cylinders using a force of 12000 lbs. These samples were prepared by spray drying a formulation comprising guanidine nitrate, basic copper nitrate, biguanide formamide copper nitrate and glass fibers. Aluminum hydroxide of different particle sizes was then mixed into the spray-dried formulation and pressed into 0.5 x 0.43" diameter cylinders. The cylinders were then burned in a 1 liter closed tank under 3000 psi nitrogen. Altho...
example 2
[0067] The gas generants of Comparative Examples 1 and 2 described in the Background of Example 1 were also compressed into 0.25" diameter x 0.060" sheets, loaded into the driver's side automotive air bag inflator, and deployed in a 60 liter water tank middle. After deployment, the tank is flushed, and the wash water is collected. Insoluble particulates were captured on a filter and weighed after drying. Any soluble particulates were precipitated by evaporating the wash water and weighed. The total particulate escaping from the combustion filter was determined by adding together the weights of soluble and insoluble particulate found in the tank. This value is called the "tank wash value".
[0068] In Table 3 the water washout values of the gas generants from Comparative Example 1 and Example 2 are given.
[0069]
Comparative example 1
Example 2
Washing value (g)
2.5-3.9
0.5-0.9
[0070] table 3
[0071] As shown in Table 3, comp...
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