Permeable crosslinked concrete protective paint and preparation method thereof
A protective coating and concrete technology, applied in the direction of coating, can solve the problems of limited hydraulic concrete application, unsatisfactory coating adhesion, failure of protective effect, etc. knotty effect
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Embodiment 1
[0025] In Example 1 and Example 2, the polysiloxane-epoxy resin used is prepared from polymethylphenylsiloxane, modified hydrogenated bisphenol A type epoxy resin and organotin catalyst, Its synthesis is carried out as follows: (1) preparation of modified hydrogenated bisphenol A type epoxy resin: 1. according to the mass ratio of each component: hydrogenated bisphenol A type epoxy resin: polyethylene glycol PEG1000:25wt% The aqueous sodium hydroxide solution=20:10:1, select hydrogenated bisphenol A type epoxy resin, macrogol PEG1000 and sodium hydroxide aqueous solution; 2. Hydrogenated bisphenol A type epoxy resin and polyethylene glycol are in three ports Mix in the flask, and heat to 70°C until the two are melted, then add 25wt% sodium hydroxide aqueous solution dropwise to the three-necked flask, and control the temperature at 70°C for 3 hours to obtain the modified hydrogenated bisphenol A ring Oxygen resin; (2) polysiloxane-epoxy resin synthesis: ① according to the mass...
Embodiment 3
[0026] In Example 3 and Example 4, the polysiloxane-epoxy resin used is prepared from polymethylphenylsiloxane, modified hydrogenated bisphenol A type epoxy resin and organotin catalyst, Its synthesis is carried out as follows: (1) preparation of modified hydrogenated bisphenol A type epoxy resin: 1. according to the mass ratio of each component: hydrogenated bisphenol A type epoxy resin: polyethylene glycol PEG1000:25wt% The aqueous sodium hydroxide solution=20:10:1, select hydrogenated bisphenol A type epoxy resin, macrogol PEG1000 and sodium hydroxide aqueous solution; 2. Hydrogenated bisphenol A type epoxy resin and polyethylene glycol are in three ports Mix in the flask, and heat to 70°C until the two are melted, then add 25wt% sodium hydroxide aqueous solution dropwise to the three-necked flask, and control the temperature at 70°C for 3 hours to obtain the modified hydrogenated bisphenol A ring Oxygen resin; (2) polysiloxane-epoxy resin synthesis: 1. according to the mas...
Embodiment 5
[0027]In Example 5 and Example 6, the polysiloxane-epoxy resin used is prepared from polymethylphenylsiloxane, modified hydrogenated bisphenol A type epoxy resin and organotin catalyst, Its synthesis is carried out as follows: (1) preparation of modified hydrogenated bisphenol A type epoxy resin: 1. according to the mass ratio of each component: hydrogenated bisphenol A type epoxy resin: polyethylene glycol PEG1000:25wt% The aqueous sodium hydroxide solution=20:10:1, select hydrogenated bisphenol A type epoxy resin, macrogol PEG1000 and sodium hydroxide aqueous solution; 2. Hydrogenated bisphenol A type epoxy resin and polyethylene glycol are in three ports Mix in the flask, and heat to 70°C until the two are melted, then add 25wt% sodium hydroxide aqueous solution dropwise to the three-necked flask, and control the temperature at 70°C for 3 hours to obtain the modified hydrogenated bisphenol A ring Oxygen resin; (2) polysiloxane-epoxy resin synthesis: ① according to the mass ...
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