Low-temperature gas-phase multi-element strengthening method preset with three-stage process

A method of gas and low temperature technology, which is applied in the field of low temperature preset three-stage gas phase multiple strengthening, can solve the problems of poor quality stability, narrow application temperature range, high cost, etc., achieve anti-oxidation, energy saving and environmental protection, pollution-free green treatment, and improve The effect of hardness

Active Publication Date: 2016-10-26
赵海军
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These methods all have shortcomings such as single infiltration element, long time, shallow infiltration layer, high cost and poor quality stability, narrow application temperature range (generally 500-590°C) and serious environmental pollution (such as QPQ). At present, the national "Industrial Structure Adjustment Catalog" has clarified that salt solution soft nitriding (QPQ belongs to the restricted category) is a restricted process range

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] A low-temperature preset three-stage gas phase multiple strengthening method, comprising the following steps:

[0025] (1) Sandblast or pickle the workpiece to be processed, and then put it into the fixture;

[0026] (2) Put the fixture into the heating furnace for heat treatment:

[0027] (21) Raise the temperature in the heating furnace to 350°C, keep it warm for 20-30 minutes, then raise the temperature, and at the same time pass ammonia gas into the heating furnace;

[0028] (22) When the temperature rises to 500-560°C, feed ammonia gas and penetrating agent A into the heating furnace, keep it warm for 1-3 hours and then continue to heat up;

[0029] (23) When the temperature rises to 570-670°C, feed ammonia gas and penetrating agent A into the heating furnace again, keep it warm for 0.5-1.5 hours, and then lower the temperature;

[0030] (24) When the temperature drops to 500-520°C, pass ammonia gas and penetrating agent B into the heating furnace, keep it warm f...

Embodiment 2

[0034] A low-temperature preset three-stage gas phase multiple strengthening method, comprising the following steps:

[0035] (1) Sandblast or pickle the workpiece to be processed, and then put it into the fixture;

[0036] (2) Put the fixture into the heating furnace for heat treatment:

[0037] (21) Raise the temperature in the heating furnace to 350°C, keep it warm for 20-30 minutes, then raise the temperature, and at the same time pass ammonia gas into the heating furnace;

[0038] (22) When the temperature rises to 500-560°C, feed ammonia gas and penetration agent A into the heating furnace, keep it warm for 1-3 hours, and then continue to heat up;

[0039] (23) When the temperature rises to 570-670°C, feed ammonia gas and penetrating agent A into the heating furnace again, keep it warm for 0.5-1.5 hours, and then lower the temperature;

[0040] (24) When the temperature drops to 500-520°C, pass ammonia gas and penetrating agent B into the heating furnace, keep it warm ...

Embodiment 3

[0044] A low-temperature preset three-stage gas phase multiple strengthening method, comprising the following steps:

[0045] (1) Sandblast or pickle the workpiece to be processed, and then put it into the fixture;

[0046] (2) Put the fixture into the heating furnace for heat treatment:

[0047] (21) Raise the temperature in the heating furnace to 350°C, keep it warm for 20-30 minutes, then raise the temperature, and at the same time pass ammonia gas into the heating furnace;

[0048] (22) When the temperature rises to 500-560°C, feed ammonia gas and penetration agent A into the heating furnace, keep it warm for 1-3 hours, and then continue to heat up;

[0049] (23) When the temperature rises to 570-670°C, feed ammonia gas and penetrating agent A into the heating furnace again, keep it warm for 0.5-1.5 hours, and then lower the temperature;

[0050] (24) When the temperature drops to 500-520°C, pass ammonia gas and penetrating agent B into the heating furnace, keep it warm ...

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PUM

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Abstract

The invention discloses a low-temperature gas-phase multi-element strengthening method preset with a three-stage process. The low-temperature gas-phase multi-element strengthening method preset with the three-stage process comprises the following steps: (1) performing sand blasting or pickling on a to-be-treated workpiece, and putting the to-be-treated workpiece subjected to sand blasting or pickling into a clamp; (2) putting the clamp into a heating furnace for heat treatment: (21) increasing a temperature in the heating furnace to 350 DEG C, preserving the heat for 20-30 minutes, warming, and introducing ammonia gas into the heating furnace; (22) when the temperature is increased to 500-560 DEG C, introducing ammonia gas and a permeating agent A into the heating furnace, preserving the heat for 1-3 hours and continuously warming; (23) when the temperature is increased to 570-670 DEG C, introducing the ammonia gas and the permeating agent A into the heating furnace again, preserving the heat for 0.5-1.5 hours, and cooling; and (24) when the temperature is reduced to 500-520 DEG C, introducing ammonia gas and a permeating agent B into the heating furnace, preserving the heat for 1-3 hours, and then, cooling and discharging. The low-temperature gas-phase multi-element strengthening method preset with the three-stage process solves the problem that temperature range is relatively narrow, and can carry out alpha-Fe high-temperature-section surface modifying and strengthening treatment at a temperature being 500-670 DEG C.

Description

technical field [0001] The invention belongs to the field of heat treatment, and in particular relates to a low-temperature preset three-stage gas phase multiple strengthening method. Background technique [0002] At present, low-temperature chemical heat treatment adopts: nitriding, nitrocarburizing, liquid nitrocarburizing (such as QPQ), etc. These methods all have shortcomings such as single infiltration element, long time, shallow infiltration layer, high cost and poor quality stability, narrow application temperature range (generally 500-590°C) and serious environmental pollution (such as QPQ). At present, the national "Industrial Structure Adjustment Catalogue" has specified that salt solution soft nitriding (QPQ belongs to the restricted category) is a restricted process range. Contents of the invention [0003] In order to improve the above-mentioned problems, the object of the present invention is to provide a low-temperature preset three-stage gas-phase multi-co...

Claims

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Application Information

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IPC IPC(8): C23C12/00
CPCC23C12/00
Inventor 赵明明赵海军
Owner 赵海军
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