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A preparation method of in-situ synthesis of multi-component multi-scale carbide reinforced iron-based wear-resistant coating

An in-situ synthesis and wear-resistant coating technology, which is applied in the field of wear-resistant coatings, can solve problems such as the mismatch between the reinforcing phase and the wear resistance of the substrate, and achieve the effects of simple and convenient equipment, good compatibility, and large specific surface area

Active Publication Date: 2018-07-20
CHINA THREE GORGES UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

It not only solves the mismatch between the reinforcement phase and the wear resistance of the matrix, but also improves the toughness of the coating

Method used

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  • A preparation method of in-situ synthesis of multi-component multi-scale carbide reinforced iron-based wear-resistant coating
  • A preparation method of in-situ synthesis of multi-component multi-scale carbide reinforced iron-based wear-resistant coating
  • A preparation method of in-situ synthesis of multi-component multi-scale carbide reinforced iron-based wear-resistant coating

Examples

Experimental program
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specific Embodiment

[0039] Process the substrate into a tool or mold that meets the requirements of use, and clean the grease on the surface with acetone; if the substrate is remanufactured as a failed component, it needs to be sandblasted on the surface, and the grease on the surface is cleaned with acetone; A good substrate is put into the workpiece table and fixed.

[0040] The following three examples are used to complete the preparation of the in-situ synthesis of multiple multi-scale and multi-scale carbide composite reinforced coatings on the surface of the substrate:

Embodiment 1

[0042] 40% W powder (W≥99.8%, particle size 100~150μm), 15% Cr powder (Cr≥99.0%, particle size 120~200μm), 0.45% Ti powder (Ti≥99.0; Fe≤0.25%; Si ≤0.1%; O≤0.65%, particle size 100~200μm), 5.2% C powder (C≥98%, particle size 80~150μm), the balance is Fe-Ni self-fluxing alloy powder (Ni=30%; Re =1%; Fe=69%, particle size is 100~200μm) dried and mixed evenly and loaded into the powder feeder; preheat the substrate, the preheating temperature is 150~200℃; prepare the coating by plasma cladding process , the process parameters are: arc current 70~90A, voltage 38~46V, mixed powder feeding speed 15~20g / min, ion gas flow 6~8L / min, powder feeding gas flow 3~5L / min, shielding gas flow 6~8L / min, cladding speed 45~60mm / min; while the coating is being prepared, a high-temperature aluminum silicate ceramic fiber blanket is used to keep the reaction molten pool warm. The high-temperature ceramic fiber blanket is made of high-temperature aluminum silicate ceramic fiber with a thickness of 30...

Embodiment 2

[0045] 35% W powder (W≥99.8%, particle size 100~150μm), 20% Cr powder (Cr≥99.0%, particle size 120~200μm), 0.3% Ti powder (Ti≥99.0%; Fe≤0.25%; Si≤0.1%; O≤0.65%, particle size 100~200μm), 5.8% C powder (C≥98%, particle size 80~150μm), the balance is Fe-Ni self-fluxing alloy powder (Ni=30%; Re=1%; Fe=69%, the particle size is 100~200μm) dried and mixed evenly, then loaded into the powder feeder; the substrate is preheated, the preheating temperature is 150~200℃; the coating is prepared by plasma cladding process Layer, the process parameters are: arc current 70~90A, voltage 38~46V, mixed powder feeding speed 15~20g / min, ion gas flow 6~8L / min, powder feeding gas flow 3~5L / min, shielding gas The flow rate is 6~8L / min, and the cladding speed is 45~60mm / min; while the coating is being prepared, a high-temperature aluminum silicate ceramic fiber blanket is used to keep the reaction molten pool warm.

[0046] The obtained TiC-WC-M 7 C 3 Composite reinforced iron-based coatings were...

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Abstract

The invention relates to the field of abrasion-resistant coatings, in particular to a method for preparing multi-element and multi-scale carbide enhanced iron-based abrasion-resistant coating through in-situ synthesis. The method comprises steps as follows: alloy powder containing W powder, Cr powder, Ti powder, C powder and Fe-Ni powder is sent into a preheated substrate; then the mixed alloy powder is heated and molten by argon plasma, and the abrasion-resistant coating is obtained through an in-situ reaction. Carbides generated with the method have a multi-element and multi-scale texture structure, the structure can overcome limitation of the single-scale carbide during enhancement, the multi-scale carbides learn from others' strong points, offset own weakness and are complementary in hardness and toughness to produce a compound enhancement effect on the substrate, and accordingly, the problems that the single enhancing phase and the substrate abrasion rate are not matched and the toughness is reduced are solved.

Description

technical field [0001] The invention relates to the field of wear-resistant coatings, in particular to a preparation method for in-situ synthesis of multi-element and multi-scale carbide reinforced iron-based wear-resistant coatings. Background technique [0002] Metal-based carbide coating is an important wear-resistant material, in which the metal phase is the binder and the carbide is the reinforcing phase. Due to the strong covalent bond of carbide, it has high hardness, high melting point, high chemical stability, wear resistance, corrosion resistance and other properties, and is widely used in the manufacture of cemented carbide tools, drills, mold edges, etc. . However, carbides rarely exist in nature and need to be synthesized artificially. The in-situ synthesis method can directly obtain carbides in the matrix material through in-situ chemical reactions at one time. Since the carbides are nucleated in the matrix metal and grow spontaneously, there is no pollution ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C24/10
CPCC23C24/103
Inventor 袁有录
Owner CHINA THREE GORGES UNIV