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Method for thermally measuring heat insulation amount at high temperature and high pressure

A kind of adiabatic heat, high temperature and high pressure technology, used in the field of adiabatic heat measurement under high temperature and high pressure

Inactive Publication Date: 2017-01-04
CHINA PETROLEUM & CHEM CORP +1
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0007] The technical problem to be solved by the present invention is that there is no method for adiabatic calorimetry measurement under high temperature and high pressure in the prior art, and a new method for adiabatic calorimetry measurement under high temperature and high pressure is provided

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  • Method for thermally measuring heat insulation amount at high temperature and high pressure
  • Method for thermally measuring heat insulation amount at high temperature and high pressure
  • Method for thermally measuring heat insulation amount at high temperature and high pressure

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Embodiment 1

[0024] The present invention provides a method capable of performing calorimetric testing below 800°C and below 20MPa. The calorimetric method can perform calorimetric measurement according to the adiabatic mode and isothermal mode, can implement precise control over the reaction process and can collect and analyze data in real time .

[0025] The device is mainly composed of the following parts (such as figure 1 shown):

[0026] Central control system: generally consists of a signal acquisition card, a digital-to-analog converter and pre-programmed computer software.

[0027] Pressure control unit: connected to the compensation gas (usually nitrogen) gas source, through the opening and closing of the solenoid valve to control the compensation pressure in the kettle;

[0028] Temperature control unit: control the start-stop and power of the heating and heat preservation unit so that the actual temperature conforms to the set value;

[0029] Reactor (which is the key part of t...

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Abstract

The invention relates to a method for thermally measuring the heat insulation amount at high temperature and high pressure. The method mainly solves the problem that a method for thermally measuring the heat insulation amount at high temperature and high pressure is not available in the prior art. According to the method for thermally measuring the heat insulation amount at high temperature and high pressure, a calorimetry test can be carried out on a device for thermally measuring the heat insulation amount according to a heat insulation mode and an isothermy mode at the temperature below 800 DEG C and the pressure below 20 MPa, the reaction process can be precisely controlled, and data can be acquired and analyzed in real time. According to the technical scheme, the device comprises a central control system, a pressure control unit, a temperature control unit and a reaction still, the problems are well solved, and method can be used for thermally measuring the heat insulation amount at high temperature and high pressure.

Description

technical field [0001] The invention relates to a method for adiabatic calorimetry under high temperature and high pressure. Background technique [0002] To evaluate the thermal risk of a specific process, it is necessary to obtain parameters such as heat release rate, heat release, adiabatic temperature rise, and adiabatic pressure rise, and these parameters must be obtained through calorimetric testing. The modes of operation of the calorimeter include isothermal, dynamic and adiabatic. Commonly used calorimeters mainly include reaction calorimeter (RC1), accelerating rate calorimeter (ARC) and adiabatic calorimeter (Accelerating Rate Calorimeter and Method of Operation, US4208907), differential scanning calorimeter (DSC), etc. [0003] For the calorimetric test for the purpose of process thermal risk assessment, the following conditions are often required: 1) The sample size is large enough to reduce the influence of the amplification effect; 2) Because the adiabatic mo...

Claims

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Application Information

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IPC IPC(8): G01N25/20
CPCG01N25/20
Inventor 金满平孙冰朱红伟姜杰徐伟
Owner CHINA PETROLEUM & CHEM CORP
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