Method for preparing organic calcium with eggshells

An organic calcium and eggshell technology, applied in the fields of application, food science, food ingredients, etc., can solve the problems of inability to meet the demand for calcium supplementation, calculus and constipation, unsuitable for taking, etc., and achieve low price, promote absorption, and promote formation. Effect

Inactive Publication Date: 2017-01-11
邵玉华
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This patented technology allows for easy-to-produce organocalcium with improved purity compared to existing methods that require complicated steps or expensive materials. It involves extracting it through an aqueous phase containing water soluble calcium salt (CaCl2) dissolved therein without damaging any other components like albumen). By adding protetronic acids before grinding off the shells, excessive amounts of calciuminous chloride may also get mixed together during processing. After this treatment, the resulting liquor has higher levels of free lime permeability than previously possible due to its composition. Additionally, the extracted material includes smaller quantities of calciumen trihydroxypropylheptanoidone diphosphatite) while still being effective at promoting intestinal uptake of nutrients such as phytonutritional agents. Overall, these technical results lead to more pure and useful organochelctrochemistry products made up entirely from recovered egg shards.

Problems solved by technology

This patented technical problem addressed by this patents relates to finding an improved way to make better use of existing sources like eggs or other animal products that contain valuable mineral resources (such as calciium).

Method used

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Examples

Experimental program
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Effect test

Embodiment 1

[0019] A method for preparing organic calcium from eggshells, specifically comprising the following steps:

[0020] (1) Crushing: Wash and break the eggshells, pass through a 100-mesh sieve, add distilled water twice the weight of the eggshells, mix well, heat to 71°C, homogenize at 33MPa for 60 seconds, then homogenize at 14MPa for 30 seconds , cooled to 45°C to obtain eggshell liquid;

[0021] (2) Enzymolysis: Add protease to the eggshell liquid with a mass concentration of 0.03%, place it in a constant temperature water bath at 40°C, stir at 52 rpm for 120 minutes, decompose the protein into small molecular substances, remove impurities, and obtain the enzyme Egg shell solution;

[0022] (3) Fermentation: Add glucose to the enzymatic eggshell solution to make the concentration of glucose 13%, stir until completely dissolved, sterilize at 121°C for 16 minutes, add lactic acid bacteria to make the concentration 3% (v / v) , stirred evenly, fermented at a constant temperature ...

Embodiment 2

[0029] A method for preparing organic calcium from eggshells, specifically comprising the following steps:

[0030] (1) Crushing: Wash and break the duck eggshell, pass through a 100-mesh sieve, add distilled water twice the weight of the eggshell, mix well, heat to 72°C, homogenize at 34MPa for 65 seconds, then homogenize at 15MPa for 35 seconds , cooled to 48°C to obtain eggshell liquid;

[0031] (2) Enzymolysis: Add protease to the eggshell liquid with a mass concentration of 0.04%, place it in a constant temperature water bath at 41°C, stir at 53 rpm for 130 minutes, decompose the protein into small molecular substances, remove impurities, and obtain the enzyme Egg shell solution;

[0032] (3) Fermentation: Add glucose to the enzymatic eggshell solution to make the mass concentration of glucose 14%, stir until completely dissolved, sterilize at 121°C for 17 minutes, add lactic acid bacteria to make the concentration 3% (v / v) , stirred evenly, fermented at a constant temp...

Embodiment 3

[0039] A method for preparing organic calcium from eggshells, specifically comprising the following steps:

[0040] (1) Crushing: Wash and crush the goose eggshell, pass through a 120-mesh sieve, add distilled water three times the weight of the eggshell, mix well, heat to 73°C, homogenize at 35MPa for 70 seconds, and homogenize at 16MPa for 40 seconds seconds, cooled to 50°C to obtain eggshell liquid;

[0041] (2) Enzymolysis: Add protease to the eggshell liquid with a mass concentration of 0.05%, place it in a constant temperature water bath at 42°C, stir at 54 rpm for 140 minutes, decompose the protein into small molecular substances, remove impurities, and obtain the enzyme Egg shell solution;

[0042] (3) Fermentation: Add glucose to the enzymatic eggshell solution to make the mass concentration of glucose 15%, stir until completely dissolved, sterilize at 121°C for 18 minutes, add lactic acid bacteria to make the concentration 4% (v / v) , stirred evenly, and fermented a...

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Abstract

The invention discloses a method for preparing organic calcium with eggshells. The method includes the steps of 1), breaking; 2), performing enzymolysis; 3), fermenting; 4), extracting; 5), packaging. The method for preparing the organic calcium with the eggshells is simple and efficient, large-scale production can be performed, extraction rate reaches 86.36%, content of calcium lactate is 93.62%, calcium gluconate is 5.46%, and revenue is increased by 15.6%. Residue protein can be decomposed by directly adding protease into the broken eggshells, and impurities in an eggshell solution can be reduced; the eggshell solution subjected to enzymolysis is fermented via lactic acid bacteria, macromolecular impurities are decomposed, lactic acid is produced, calcium ions in the calcium carbonate is separated out, and formation of the calcium lactate is facilitated; the solution is subjected to secondary crystallization to separate out organic calcium crystals, and extract rate of the organic calcium is increased; the abandoned eggshells are fully utilized and made profitable, low cost is achieved, cost is saved, poisonous reagents are not used during the preparation, residues of the reagent cannot be caused, and the method is healty and environment friendly.

Description

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Claims

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Application Information

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Owner 邵玉华
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