Chinese wolfberry fruit extract solid drink and preparation method thereof
A technology of wolfberry extract and solid beverage, applied in the field of health food
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Embodiment 1
[0034] 1) Weigh 1kg wolfberry leaf tea, wash with industrial water and purified water successively, pulverize, add 50% ethanol, and extract twice at 60°C for 2 hours each time. Add 10L of solvent for the first time, add 8L of solvent for the second time, centrifuge, discard the residue, and obtain the extract Ⅰ.
[0035] 2) Concentrate the extract Ⅰ to 0.6mg / mL under reduced pressure, weigh 2kg of AB-8 resin, and put it into two plexiglass resin columns with an inner diameter of 15cm and a column height of 150cm in series by wet method to form an expanded bed macroporous adsorption resin system for adsorption . The flow rate is 5BV / h (column volume, referred to as BV), and the adsorption residual liquid is discarded; after the adsorption is completed, wash with 20BV water at a flow rate of 10BV / h, and the cleaning liquid is discarded.
[0036] 3) Carry out gradient elution with 30% and 50% ethanol of 20BV successively as the eluent, the flow rate is 10BV / h, collect and combin...
Embodiment 2
[0045] 1) Weigh 10kg wolfberry leaf tea, wash with industrial water and purified water successively, pulverize, add 50% ethanol, and extract twice at 60°C for 2 hours each time. Add 100L of solvent for the first time, add 80L of solvent for the second time, centrifuge, discard the residue, and obtain the extract Ⅰ.
[0046] 2) Concentrate the extract Ⅰ to 0.6 mg / mL under reduced pressure, add 20 kg of AB-8 resin, and put two plexiglass resin columns with an inner diameter of 15 cm and a column height of 150 cm in series by wet method to form an expanded bed macroporous adsorption resin system for adsorption. The flow rate is 8BV / h (column volume, referred to as BV), and the adsorption residual liquid is discarded; after the adsorption is completed, it is washed with 20BV of water, and the flow rate is 10BV / h, and the cleaning liquid is discarded.
[0047] 3) Carry out gradient elution with 30% and 50% ethanol of 20BV successively as the eluent, the flow rate is 10BV / h, collect...
Embodiment 3
[0055] 1) Weigh 50kg wolfberry bud tea, wash with industrial water and purified water successively, pulverize, add 40% ethanol, and extract twice at 60°C for 2 hours each time. Add 500L of solvent for the first time, add 400L of solvent for the second time, centrifuge, discard the residue, and obtain the extract I.
[0056] 2) Concentrate the extract Ⅰ to 0.6 mg / mL under reduced pressure, add 100 kg of AB-8 resin, and put two plexiglass resin columns with an inner diameter of 15 cm and a column height of 150 cm in series by wet method to form an expanded bed macroporous adsorption resin system for adsorption. The flow rate is 8BV / h (column volume, referred to as BV), and the adsorption residual liquid is discarded; after the adsorption is completed, it is washed with 20BV of water, and the flow rate is 10BV / h, and the cleaning liquid is discarded.
[0057] 3) Sequentially use 20BV of 40% ethanol as the eluent to elute at a flow rate of 10BV / h, collect and combine the eluents, ...
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