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Porous polyester fiber HOY filaments and preparation method thereof

A porous polyester and fiber technology, applied in the field of polyester fiber, can solve problems such as poor mechanical properties and uneven dyeing of polyester fibers, and achieve the effects of improving processing performance, improving dyeing performance, and maintaining excellent performance

Active Publication Date: 2017-02-15
JIANGSU HENGLI CHEM FIBER
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0010] The purpose of the present invention is to overcome the problems of uneven dyeing and poor mechanical properties of existing polyester fibers, realize large-scale production and spinning, and provide a method for preparing porous polyester fiber HOY filaments

Method used

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  • Porous polyester fiber HOY filaments and preparation method thereof
  • Porous polyester fiber HOY filaments and preparation method thereof
  • Porous polyester fiber HOY filaments and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0064] A preparation method of modified polyester, specifically comprising the following steps:

[0065] (1) Preparation of glycol terephthalate:

[0066] Put terephthalic acid and 2-pentyl-1,3 propanediol with a molar ratio of 1:1.3 into a slurry and add it to the reactor at a concentration of 50 wt%, and the addition amount is 0.3% of the weight of terephthalic acid. Under the catalysis of sulfuric acid, esterification reaction is carried out. The esterification reaction is pressurized in a nitrogen atmosphere. The pressurized pressure is normal pressure and the temperature is 180°C. Time is the end point of the esterification reaction to obtain diol terephthalate;

[0067] (2) Preparation of ethylene terephthalate:

[0068] Put terephthalic acid and ethylene glycol into a slurry with a molar ratio of 1:1.2 and put them into the reactor to carry out esterification reaction. The esterification reaction is pressurized in a nitrogen atmosphere. The pressurized pressure is nor...

Embodiment 2

[0076]The preparation process of the modified polyester of embodiment 2 is the same as embodiment 1, and wherein main technical parameter is referring to table 1; After step (3) adds diol terephthalate, stirs and mixes for 16 minutes, when add-on is Under the action of 0.011% of the catalyst antimony trioxide of the total weight of terephthalic acid and the stabilizer triphenyl phosphate of 0.02% of the total weight of terephthalic acid, the low vacuum stage is started under the condition of negative pressure For the polycondensation reaction, the pressure at this stage is steadily pumped from normal pressure to an absolute pressure of 490Pa, the temperature is controlled at 262 ° C, and the reaction time is 31 minutes; then continue to vacuumize and carry out the polycondensation reaction in the high vacuum stage to reduce the reaction pressure to an absolute pressure of 90Pa. The reaction temperature was controlled at 276° C., and the reaction time was 51 minutes to prepare t...

Embodiment 3

[0079] The preparation process of the modified polyester of embodiment 3 is the same as embodiment 1, and wherein main technical parameter is referring to table 1; After step (3) adds diol terephthalate, stirs and mixes for 16 minutes, when add-on is Under the action of 0.03% of the catalyst antimony trioxide of the total weight of terephthalic acid and the stabilizer triphenyl phosphate of 0.02% of the total weight of terephthalic acid, the low vacuum stage is started under the condition of negative pressure For the polycondensation reaction, the pressure at this stage is steadily pumped from normal pressure to an absolute pressure of 498Pa, the temperature is controlled at 263°C, and the reaction time is 32 minutes; then continue to vacuumize and carry out the polycondensation reaction in the high vacuum stage, so that the reaction pressure drops to an absolute pressure of 90Pa. The reaction temperature was controlled at 277° C., and the reaction time was 57 minutes to prepar...

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Abstract

The invention relates to porous polyester fiber HOY filaments and a preparation method thereof; the porous polyester fiber HOY filaments are prepared by spinning modified polyester through a porous spinneret plate; an arrangement way of spinneret holes in the porous spinneret plate is in oval arrangement, that is to say, a hole center of the spinneret holes is located in concentric ellipses, the concentric ellipses are a series of ellipses, the long axes of all the ellipses are collinear, and the short axes are collinear. The porous polyester fiber HOY filaments are prepared by metering, extruding, cooling, oiling and high-speed coiling of the modified polyester, wherein a preparation method for the modified polyester comprises the steps: carrying out a reaction of terephthalic acid and ethylene glycol to prepare ethylene glycol terephthalate, adding terephthalic acid and branched chain-containing dihydric alcohol, carrying out a reaction to prepare dihydric alcohol terephthalate, and continuing to carry out a reaction to obtain the modified polyester. The prepared fiber is excellent in properties, the linear density deviation rate of the porous polyester fiber HOY filaments is less than or equal to 0.2%, the CV value of breaking strength is less than or equal to 2.5%, and the CV value of breaking elongation is less than or equal to 5.0%.

Description

technical field [0001] The invention belongs to the field of polyester fibers, and relates to a porous polyester fiber HOY filament and a preparation method thereof. Background technique [0002] Since its inception, polyethylene terephthalate (PET fiber or polyester fiber) fiber has high breaking strength and elastic modulus, moderate resilience, excellent heat setting, good heat resistance and light resistance, acid resistance, alkali resistance and corrosion resistance. It has a series of excellent performances, such as anti-wrinkle and non-ironing, and good crispness. It is widely used in clothing, home textiles and other fields. [0003] However, due to the high crystallinity and compact structure of PET, and there is no functional group combined with the dye on the molecular chain, it is difficult for the dye molecule to enter the fiber and dyeing is difficult. Can't satisfy people to bright-coloured beautiful, the fabric demand of unique style. [0004] The reason f...

Claims

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Application Information

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IPC IPC(8): D01F6/84C08G63/183C08G63/78D01D5/253
CPCC08G63/183C08G63/78D01D5/253D01F6/84
Inventor 范红卫尹立新陈明孙晓华金管范
Owner JIANGSU HENGLI CHEM FIBER
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