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A kind of preparation method of γ-tial base alloy bar

A technology for base alloys and rods, which is applied in the field of preparation of γ-TiAl base alloy rods, can solve problems such as limited application prospects, complicated process flow, and poor operability, and achieve simple sheath structure, reduced costs, and reduced the formation of the effect

Active Publication Date: 2018-02-13
NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, many scholars have researched different sheath design schemes, such as placing or pasting titanium plates or precious metal plates on the inner lining of the sheath, or putting in a glass fiber insulation layer, or vacuuming the space between the sheath and the blank, etc. These technological processes Complicated, poor operability and high cost, or only limited to the processing of small samples, the application prospects are limited
At present, the domestic TiAl alloy mostly adopts a multi-layer sheath structure with an increased isolation layer. For example, a fiber layer is added to the outer sheath to prevent temperature drop, and the fiber layer is mostly made by hand, which has poor stability, and the fiber material is harmful to the human body. Hazardous; or some add pure titanium plates for insulation, the process is complicated and the cost is high

Method used

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  • A kind of preparation method of γ-tial base alloy bar
  • A kind of preparation method of γ-tial base alloy bar

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] The preparation of γ-TiAl-based alloy rods in this embodiment includes the following steps:

[0029] Step 1. Obtain gamma-TiAl alloy ingots through vacuum melting three times by vacuum melting method. The nominal composition of the alloy ingots is Ti-45Al-3Ta-2Cr-0.2W. The diameter of the alloy ingots is 120mm, and the The TiAl alloy ingot is peeled, riser cut and trimmed;

[0030] Step 2, making a bag with a diameter of 156mm, such as figure 1 As shown, the wrapper includes a wrapper sleeve 1 and two wrapper covers 2 for sealing two ports of the wrapper sleeve 1, and the wrapper cover 2 is provided with vent holes 3; the wrapper sleeve 1 has a thickness of 15mm, and the thickness of the wrapping cover 2 is 20mm; the material of the wrapping sleeve 1 and the wrapping cover 2 is stainless steel;

[0031] Step 3. In step 2, one end of the wrapping sleeve 1 is welded with one of the wrapping caps 2 to form a cylinder. After the cylinder is heat-preserved for 0.8 hours at...

Embodiment 2

[0037] The preparation of γ-TiAl-based alloy rods in this embodiment includes the following steps:

[0038] Step 1. Obtain gamma-TiAl alloy ingots through vacuum melting three times by vacuum melting method. The nominal composition of the alloy ingots is Ti-45Al-3Ta-2Cr-0.2W. The diameter of the alloy ingots is 120mm, and the The TiAl alloy ingot is peeled, riser cut and trimmed;

[0039] Step 2, making a bag with a diameter of 148mm, such as figure 1 As shown, the wrapper includes a wrapper sleeve 1 and two wrapper covers 2 for sealing two ports of the wrapper sleeve 1, and the wrapper cover 2 is provided with vent holes 3; the wrapper sleeve 1 has a thickness of 12mm, and the thickness of the wrapping cover 2 is 20mm; the material of the wrapping sleeve 1 and the wrapping cover 2 is stainless steel;

[0040] Step 3. In step 2, one end of the wrapping sleeve 1 is welded with the wrapping cap 2 to form a cylinder body. After the cylinder body is heat-preserved for 0.5 h at a...

Embodiment 3

[0046] The preparation of γ-TiAl-based alloy rods in this embodiment includes the following steps:

[0047] Step 1. Obtain gamma-TiAl alloy ingots through vacuum melting three times by vacuum melting method. The nominal composition of the alloy ingots is Ti-45Al-3Ta-2Cr-0.2W. The diameter of the alloy ingots is 120mm, and the The TiAl alloy ingot is peeled, riser cut and trimmed;

[0048] Step 2, making a bag with a diameter of 140mm, such as figure 1 As shown, the wrapper includes a wrapper sleeve 1 and two wrapper covers 2 for sealing two ports of the wrapper sleeve 1, and the wrapper cover 2 is provided with vent holes 3; the wrapper sleeve 1 has a thickness of 8mm, and the thickness of the wrapping cover 2 is 17mm; the material of the wrapping sleeve 1 and the wrapping cover 2 is stainless steel;

[0049] Step 3. In step 2, one end of the sleeve 1 is welded with the sleeve cover 2 to form a cylinder. After the cylinder is heat-preserved for 1 hour at a temperature of 100...

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Abstract

The invention discloses a preparation method of a gamma-TiAl-based alloy bar. The preparation method comprises the following steps: (I) preparing a gamma-TiAl alloy ingot through a vacuum melting method; (II) manufacturing a jacket, wherein the jacket comprises a jacket cylinder and jacket covers, the jacket covers are used for sealing the two end openings of the jacket cylinder, and each jacket cover is provided with a ventilating hole; (III) thermally treating the cylinder body, subsequently coating the inner wall of the cylinder body with an oxidation-resistant coating, afterwards putting the TiAl alloy ingot in the cylinder body and finally welding each jacket cover on the corresponding open end of the cylinder body; (IV) externally coating the oxidation-resistant coating, carrying out thermal treatment, subsequently extruding in an extruder to obtain the bar, and straightening the bar by letting the bar directly pass through a straightening tube; and (V) removing the jacket on the outer surface and carrying out homogenizing annealing treatment to obtain the gamma-TiAl-based alloy bar. The problem that a TiAl intermetallic compound is relatively large in brittleness and easy to oxidize in a hot working process can be solved through the preparation method disclosed by the invention, and the prepared gamma-TiAl-based alloy bar is uniform in microstructure and high in mechanical property.

Description

technical field [0001] The invention belongs to the technical field of intermetallic compounds, and in particular relates to a method for preparing gamma-TiAl-based alloy rods. Background technique [0002] γ-TiAl intermetallic compound has the characteristics of high specific strength, specific modulus, good oxidation resistance, creep resistance, excellent high temperature strength, stiffness and low density, and has become an important candidate material for high temperature structural materials on aerospace vehicles one. However, the intrinsic brittleness and low room temperature plasticity of γ-TiAl-based alloys bring great difficulties to its processing and forming, and also restrict its wide application in structural materials. The quality of TiAl alloy preparation will be related to the comprehensive mechanical properties of the alloy, affect the development process and speed of the aviation industry, and is also a prerequisite for the industrial application of the ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C1/02B21C37/04B21C31/00C22F1/18
CPCB21C31/00B21C37/045C22C1/02C22F1/183
Inventor 罗媛媛毛小南吴金平杨帆苏航标郭荻子杨英丽
Owner NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH