Modified epoxy resin seepage-prevention and leak-stopping grouting material and method for concrete in arctic-alpine area
A technology of epoxy resin and concrete, which is applied in the field of modified epoxy resin anti-seepage plugging grout for concrete in alpine regions, can solve the problems of frequent thermal expansion and contraction, high initial viscosity, slow curing rate, etc., and meet the requirements of Engineering application requirements, guaranteed operating time, and the effect of reducing initial viscosity
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Embodiment 1
[0033] In a 250 mL four-neck flask, add 10 g of trimethoxy-terminated hydroxyl-terminated silicone oil PDMS (Mn=10000), 10 g of epoxy resin E-4490 g, add 3 drops of catalyst dibutyltin dilaurate, and heat at reflux at 120 °C for 5 h , distilled under reduced pressure until no more bubbles are produced, and the residue in the kettle is the modified epoxy resin. Get this epoxy resin 40 g, furfural acetone reactive diluent 45 g, the hydrolyzate 13 g of curing agent N-(β-aminoethyl)-γ-aminopropyltrimethoxysilane and accelerator DMP-30 2g, Stir evenly at 0 ℃ to be the grouting material. The basic properties of the grouting material are shown in Table 1.
Embodiment 2
[0035] In a 250 mL four-necked flask, add 10 g of triethoxy-terminated hydroxyl-terminated silicone oil PDMS (Mn=10000), 190 g of epoxy resin E-5190 g, add 3 drops of catalyst dibutyltin dilaurate, and heat to reflux at 120 °C for 5 h Finally, distill under reduced pressure until no bubbles are produced, and the residue in the kettle is the modified epoxy resin. Get this epoxy resin 30 g, furfural acetone reactive diluent 50 g, the hydrolyzate 18 g of curing agent N-(β-aminoethyl)-γ-aminopropyltriethoxysilane and accelerator DMP-30 2g , stirring evenly at 0 ℃ is the grouting material. The basic properties of the grouting material are shown in Table 1.
Embodiment 3
[0037] In a 250 mL four-necked flask, 10 g of trimethoxy-terminated hydroxyl-terminated silicone oil PDMS (Mn=10000), 10 g of epoxy resin E-4490 g, and 3 drops of catalyst dibutyltin dilaurate were added, and heated under reflux at 120 °C for 5 h. Distill under reduced pressure until there are no more bubbles, and the residue in the kettle is the modified epoxy resin. Get this epoxy resin 40 g, furfural acetone reactive diluent 38 g, the hydrolyzate 20 g of curing agent N-(β-aminoethyl)-γ-aminopropyltriethoxysilane and accelerator DMP-30 2g , stirring evenly at 0 ℃ is the grouting material. The basic properties of the grouting material are shown in Table 1.
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