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Oral antelope horn freeze-dried powder and processing method thereof

A processing method, technology of antelope horns, applied in the direction of freeze-drying transportation, powder transportation, pharmaceutical formulations, etc., to achieve the effect of uniform dispersion

Inactive Publication Date: 2017-07-07
泸州德高生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, there is no relevant report about oral administration of antelope horn freeze-dried powder

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] A processing method for oral antelope horn freeze-dried powder, comprising the following steps:

[0023] (1) After the antelope horns are coarsely crushed, the particle size of the antelope horns is finely crushed to nanometer level;

[0024] (2) Slowly boil the sucrose syrup water, add the antelope horn nanoparticles into the sucrose syrup, and stir to form an antelope horn sucrose mixed slurry, cool for later use;

[0025] (3) The cooled antelope horn sucrose mixed slurry is vacuum freeze-dried. The vacuum freeze-drying process is as follows: first cool down to -60°C, keep warm for 30min-40min; then cool down to -80°C, keep warm for 10min-20min; 0℃~10℃, keep warm for 30min~40min.

[0026] The crushing temperature of finely crushed powder is -70~-60℃.

[0027] In step (3), the uniform heating rate is 3-6° C. / min.

[0028] Before vacuum freeze-drying, a continuous cooling-insulation process of 6-8°C / min is required.

[0029] The heat preservation temperature in the ...

Embodiment 2

[0033] A processing method for oral antelope horn freeze-dried powder, comprising the following steps:

[0034] (1) After the antelope horns are coarsely crushed, the particle size of the antelope horns is finely crushed to nanometer level;

[0035] (2) Slowly boil the sucrose syrup water, add the antelope horn nanoparticles into the sucrose syrup, and stir to form an antelope horn sucrose mixed slurry, cool for later use;

[0036] (3) The cooled antelope horn sucrose mixed slurry is vacuum freeze-dried. The vacuum freeze-drying process is as follows: first cool down to -70°C, keep warm for 30min-40min; then cool down to -85°C, keep warm for 10min-20min; 0℃~10℃, keep warm for 30min~40min.

[0037] The crushing temperature of finely crushed powder is -70~-60℃.

[0038] In step (3), the uniform heating rate is 3-6° C. / min.

[0039] Before vacuum freeze-drying, a continuous cooling-insulation process of 6-8°C / min is required.

[0040] The heat preservation temperature in the ...

Embodiment 3

[0044] A processing method for oral antelope horn freeze-dried powder, comprising the following steps:

[0045] (1) After the antelope horns are coarsely crushed, the particle size of the antelope horns is finely crushed to nanometer level;

[0046] (2) Slowly boil the sucrose syrup water, add the antelope horn nanoparticles into the sucrose syrup, and stir to form an antelope horn sucrose mixed slurry, cool for later use;

[0047] (3) The cooled antelope horn sucrose mixed slurry is vacuum freeze-dried. The vacuum freeze-drying process is as follows: first cool down to -65°C, keep warm for 30min-40min; then cool down to -80°C, keep warm for 10min-20min; 0℃~10℃, keep warm for 30min~40min.

[0048] The crushing temperature of finely crushed powder is -70~-60℃.

[0049] In step (3), the uniform heating rate is 3-6° C. / min.

[0050] Before vacuum freeze-drying, a continuous cooling-insulation process of 6-8°C / min is required.

[0051] The heat preservation temperature in the ...

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PUM

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Abstract

The invention discloses a process for producing oral antelope horn freeze-dried powder. The process comprises the following steps: coarsely crushing antelope horns, and finely crushing the antelope horns to nano scale; boiling cane syrup water over soft fire, adding the antelope horn nano particles into the cane syrup, stirring to obtain antelope horn and cane mixed syrup, and cooling for later use; and performing vacuum freeze drying on the cooled antelope horn and cane mixed syrup. The vacuum freeze drying step is as follows: cooling to -60 to -70 DEG C, and preserving the heat for 30-40 min; then cooling to -80 to -85 DEG C, and preserving the heat for 10-20 min; and uniformly heating to 0 to 10 DEG C, and preserving the heat for 30-40 min. Further disclosed is oral antelope horn freeze-dried powder, which is a solid having a porous structure.

Description

technical field [0001] The invention relates to the field of freeze-dried powder, in particular to an oral antelope horn freeze-dried powder and a processing method thereof. Background technique [0002] Antelope horn, the name of traditional Chinese medicine. This product is the horn of the male bovid saiga antelope, which is now replaced by the horn of the Tibetan antelope. Antelope horn has the effects of calming the liver and calming the wind, clearing the liver and improving eyesight, dispersing blood and detoxifying. It is often used for liver wind internal agitation, convulsions, convulsions, pregnancy eclampsia, convulsions due to high fever, epilepsy, dementia, headache, dizziness, conjunctival congestion, hyperthermic poisonous spots, carbuncles and sores. [0003] At present, there is no relevant report about oral administration of antelope horn freeze-dried powder. Contents of the invention [0004] The invention provides an orally lyophilized antelope horn ...

Claims

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Application Information

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IPC IPC(8): A61K35/32A61K9/19A61K47/26A61P25/00A61P29/00A61P1/08A61P27/02A61P25/08
CPCA61K9/0053A61K9/19A61K35/32A61K47/26
Inventor 高庆凌
Owner 泸州德高生物科技有限公司
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