A permanent magnet material with high temperature resistance and high magnetic performance
A permanent magnetic material and high magnetic technology, applied in the direction of magnetic materials, magnetic objects, electrical components, etc., can solve the problems of poor bonding between magnetic powder and special resin, unsatisfactory high temperature resistance, and easy agglomeration of special resin, etc., to achieve compensation The effects of low operating temperature, enhanced mechanical properties, and improved temperature resistance
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Embodiment 1
[0021] (1) Magnetic powder surface coupling: 100 parts by weight of Nd 2 Fe 14 B magnetic powder and 0.2 weight parts of graphene oxide powder are stirred and mixed evenly to form mixed magnetic powder; then 0.1 weight part of titanate coupling agent NDZ401 and 30 weight parts of xylene organic solvent are added to 100.2 weight parts of magnetic powder, Mix the above solution evenly through high-speed shear stirring at a speed of 2000 rpm for 0.5h, and oscillate with ultrasonic wave for 0.5h so that the magnetic powder and coupling agent can be fully mixed, and then heat the mixture while stirring until the solvent is volatilized. The modified mixed magnetic powder is dried and ground for use; (2) then the modified mixed magnetic powder is mixed with 0.1 parts by weight of ferrocene magnetic powder, dried, and then 1 part by weight of bisphenol A epoxy resin is mixed with Add the mixture of acetone to the dried mixed magnetic powder, stir at a stirring speed of 2000 rpm for 0...
Embodiment 2
[0025] (1) Magnetic powder surface coupling: 100 parts by weight of Nd 2 Fe 14 B magnetic powder and 3 parts by weight of graphene oxide powder are stirred and mixed evenly to form mixed magnetic powder, 2 parts by weight of titanate coupling agent NDZ401 and alcohol of 35 parts by weight are added to 103 parts by weight of mixed magnetic powder, passed through 500 Mix the above solution evenly with high-speed shear stirring at a speed of rpm for 1 hour, and oscillate for 1 hour to make the mixed magnetic powder and coupling agent fully mixed, and then heat the mixture while stirring until the solvent is volatilized, and the modified (2) then mix the modified mixed magnetic powder with 0.3 parts by weight of ferrocene magnetic powder, dry, then mix 6.5 parts by weight of bisphenol A epoxy resin with organic solvent acetone Add the mixed solution to the surface-coupled mixed magnetic powder, stir at a stirring speed of 500-2000 rpm for 1 hour, mix the above mixed solution even...
Embodiment 3
[0029] (1) Magnetic powder surface coupling: 100 parts by weight of Nd 2 Fe 14B magnetic powder and 2 weight parts of graphene oxide powder are stirred and mixed evenly to form mixed magnetic powder, and 5 weight parts of titanate coupling agent NDZ401 and 30 weight parts of xylene are added to 102 weight parts of mixed magnetic powder. High-speed shear stirring at 800 rpm for 1.5 hours Mix the above solution evenly, and oscillate ultrasonically for 1.5 hours so that the mixed magnetic powder and coupling agent can be fully mixed, and then heat the mixture while stirring until the solvent is volatilized. The modified mixed magnetic powder is dried and ground for use; (2) then the modified mixed magnetic powder is mixed with 0.2 parts by weight of ferrocene magnetic powder, dried, and then mixed with bisphenol A epoxy resin and organic solvent acetone Add liquid to the mixed magnetic powder after surface coupling, stir at a stirring speed of 500 ~ 2000 rpm for 1.5h to mix the ...
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