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A kind of preparation method of silicon carbide porous ceramic filter membrane material

A technology of porous ceramics and filter membranes, which is applied in the field of preparation of silicon carbide porous ceramic filter membrane materials, which can solve the problems of poor filtration effect of filter membranes and easy entry of filter membrane slurry due to particles, so as to avoid detachment and reduce pressure drop , Reduce the effect of filter pressure drop

Active Publication Date: 2020-05-19
山东赛利科膜科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The technical problem to be solved by the present invention is: in the preparation process of the traditional silicon carbide porous ceramic filter membrane material, the filter membrane slurry is easy to enter the pores of the support material due to the particles, resulting in poor filtration effect of the filter membrane. A kind of preparation method of silicon carbide porous ceramic filter membrane material

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0022]Weigh 100g of kaolin, 200g of quartz stone, and 600g of potassium feldspar in turn, pour them into a ball mill, add zirconia ball milling beads according to the mass ratio of the ball to material at 10:1, mill for 24 hours, and pass through a 325-mesh sieve after ball milling to obtain ceramic bonded 300g of cryolite, 80g of alumina, and 30g of carbon fiber were weighed in turn, poured into a ball mill, and added zirconia ball milling beads according to the mass ratio of the ball to material at 10:1, and the ball mill was treated for 3 hours, and then the materials in the ball mill were transferred into an oven , dried at a temperature of 105°C to a constant weight to obtain a dried product, and then hot-pressed the obtained dried product at a pressure of 15MPa and a temperature of 120°C to form a thin sheet with a thickness of 2mm to obtain an intermediate layer material; Add 200g of silicon carbide particles with a particle size of 200μm and 15mL of a 3% sodium carboxym...

example 2

[0025] Weigh 120g of kaolin, 220g of quartz, and 650g of potassium feldspar in turn, pour them into a ball mill, add zirconia ball milling beads according to the mass ratio of the ball to material at 20:1, mill for 36 hours, and pass through a 500-mesh sieve after ball milling to obtain ceramic bonded 500g of cryolite, 100g of alumina, 40g of carbon fiber, and 600g of absolute ethanol were weighed in turn, poured into a ball mill, and added zirconia ball milling beads according to the mass ratio of the ball to material at 20:1, ball milled for 5 hours, and then put into the ball mill Transfer the material into an oven and dry it at a temperature of 110°C until it reaches a constant weight to obtain a dried product. Then, the obtained dried product is hot-pressed into a thin sheet with a thickness of 4mm at a pressure of 20 MPa and a temperature of 160°C to obtain an intermediate layer. Materials: Add 300g of silicon carbide particles with a particle size of 300 μm and 30mL of 5...

example 3

[0028] Weigh 110g of kaolin, 210g of quartz stone, and 625g of potassium feldspar in turn, pour them into a ball mill, add zirconia ball milling beads according to the mass ratio of the ball to material at 15:1, mill for 30 hours, and pass through a 412-mesh sieve after ball milling to obtain ceramic bonded powder; weigh 400g cryolite, 90g alumina, and 35g carbon fiber in turn, pour them into a ball mill, add zirconia ball milling beads according to the mass ratio of the ball to material at 15:1, mill for 4 hours, and then transfer the materials in the ball mill to an oven , dried at a temperature of 108°C to a constant weight to obtain a dried product, and then hot-pressed the obtained dried product at a pressure of 18MPa and a temperature of 140°C to form a thin sheet with a thickness of 3mm to obtain an intermediate layer material; Add 250g of silicon carbide particles with a particle size of 250μm and 22mL of a 4% sodium carboxymethyl cellulose solution to the three-necked ...

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PUM

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Abstract

The invention belongs to the technical field of environmental protection materials, and specifically relates to a silicon carbide porous ceramic filter membrane material preparing method. The method in the invention comprises first dispersing silicon carbide powder and ceramic adhesive powder in a sodium carboxy methylcellulose solution, then curtain coating a sizing agent on a middle layer material surface made of cryolite, aluminium oxide, and carbon fiber, then sintering same at the protection state of nitrogen, performing fusion electrolysis on cryolite and aluminium oxide at high temperature, to generate oxygen, and form a porous middle layer; during the cooling and solidifying procedure, fixedly connecting, by the middle layer, an upper layer filter membrane and a lower support body to finally dissolve and remove aluminum generated after electrolysis in the middle layer by means of soaking by acetum so that the gap structure is rich, the pressure drop of the obtained filter membrane during usage is reduced, and power consumption is saved, thereby effectively solving the problem of a traditional silicon carbide porous ceramic filter membrane during the preparing process that the filter membrane sizing agent is in the form of particles so that it would easily enter void spaces in the support body material.

Description

technical field [0001] The invention belongs to the technical field of environmental protection materials, and in particular relates to a preparation method of a silicon carbide porous ceramic filter membrane material. Background technique [0002] The utilization of energy is mainly obtained through direct combustion. Due to the restriction of the existing technology, the combustion is insufficient, not only the energy utilization efficiency is low, but also a large amount of dust is emitted, which seriously pollutes the environment. Improving energy efficiency and reducing dust emissions are important research directions in materials science. Ceramic filter tubes are widely used in high-temperature gas dust removal and purification technology, and have become key components for gas-solid separation, energy saving and environmental protection in materials, metallurgy, chemical industry, electric power and other industries. Traditional high-strength and high-temperature-res...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B38/08C04B35/565C04B35/622C04B35/63C04B35/634C04B35/44C04B35/80C04B35/64C04B38/00C04B41/87B01D46/54
CPCB01D46/0001B01D46/543B01D2273/20C04B35/44C04B35/565C04B35/622C04B35/6316C04B35/6365C04B35/64C04B35/803C04B38/0087C04B38/061C04B38/08C04B41/009C04B41/5059C04B41/87C04B2235/3217C04B2235/422C04B2235/5248C04B2235/6586C04B2235/666C04B41/4535
Inventor 郭迎庆许丽君李雪晴
Owner 山东赛利科膜科技有限公司