A kind of preparation method of lambda-cyhalothrin nanopesticide
A technology of lambda-cyhalothrin and nano-pesticides, applied in botany equipment and methods, preservation of human or animal bodies, insecticides, etc., to achieve the effects of less pollution, reduced dosage, and low cost
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Embodiment 1
[0019] According to the mass ratio of the drug to the amphiphilic copolymer as 1:5, 2% of lambda-cyhalothrin was added to the dichloromethane solution of 0.5-10% chitosan-polylactic acid graft copolymer, and the ultrasonic wave was completely After dissolving, add dropwise into 1% polyvinyl alcohol (PVA) solution (the volume ratio of the two solutions is 1:10), stir at a speed of 500r / min for 10min, and ultrasonically break the mixture for 5min to obtain oil-in-water (W / O) The emulsion is obtained by rotary evaporation to remove the organic solvent to prepare a nano-preparation of 80-150nm lambda-cyhalothrin with a drug loading of 10-30%, and the encapsulation rate is greater than 75%. The nano-preparation can also be centrifuged and freeze-dried to obtain a solid nano-preparation of lambda-cyhalothrin.
[0020] The nano-pesticides prepared in this example have smaller and more uniform particle sizes, better permeability, and a certain slow-release effect, which prolongs the d...
Embodiment 2
[0022] Accurately weighed lambda-cyhalothrin and chitosan-polylactic acid graft copolymer were dissolved in acetone, respectively, and ultrasonically dissolved to prepare acetone solutions with concentrations of 1 mg / mL and 10 mg / mL, respectively. Mix according to the mass ratio of the drug to the amphiphilic copolymer at 1:5, drop into 10mL of deionized water, stir at a speed of 500r / min for 10min, stir evenly to form a drug-loaded micellar solution with protein light, and rotate to evaporate the organic solvent Finally, a nano-preparation of 60-130nm lambda-cyhalothrin with a drug load of 20-40% is prepared, and the encapsulation rate is greater than 80%. The nano-preparation can also be centrifuged and freeze-dried to obtain a solid nano-preparation of lambda-cyhalothrin.
[0023] The nano-pesticides prepared in this example have smaller and more uniform particle sizes, better permeability, and a certain slow-release effect, which prolongs the duration of pyrethroid pestici...
Embodiment 3
[0025] According to the mass ratio of the drug to the amphiphilic copolymer as 1:50, 4% lambda-cyhalothrin was added to the chloroform solution of 1-10% chitosan-polylactic acid graft copolymer, and the ultrasonic wave was completely After dissolving, add dropwise into 1% polyvinyl alcohol (PVA) solution (the volume ratio of the two solutions is 1:10), stir at a speed of 600r / min for 8min, and ultrasonically crush the mixture for 3min to obtain oil-in-water (W / O) The emulsion is obtained by rotary evaporation to remove the organic solvent to prepare a nano-preparation of 70-120nm lambda-cyhalothrin with a drug loading of 15-40%, and the encapsulation rate is greater than 85%. The nano-preparation can also be centrifuged and freeze-dried to obtain a solid nano-preparation of lambda-cyhalothrin.
[0026] The nano-pesticides prepared in this example have smaller and more uniform particle sizes, better permeability, and a certain slow-release effect, which prolongs the duration of...
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