an antibacterial dressing
A nano-titanium dioxide, fixed time technology, applied in antifouling/underwater coatings, biocide-containing paints, coatings, etc., can solve the problems of easy falling off, easy to get dust, short antibacterial time, etc., and achieve good thermal stability. and dispersibility, improving the antibacterial performance, and improving the photocatalytic performance.
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Embodiment 1
[0029] Preparation of nano-titanium dioxide sol:
[0030] (1) Mix 20 parts by mass of isopropanol with 30 parts by mass of deionized water, add sulfuric acid, control its concentration to be 0.3mol / L, and stir for 3 minutes;
[0031] (2) Add n-butyl titanate to the above solution, control its concentration to 0.1mol / L, adjust the pH between 2 and 4, continue stirring for 20 minutes, and record the mixed solution as C solution;
[0032] (3) Mix 20 parts by mass of potassium fluotitanate and 50 parts by mass of absolute ethanol, add the mixed solution into the C solution, control the addition rate to 3ml / min, and stir for 2 hours;
[0033] (4) The nano-titanium dioxide particles obtained in step (3) are separated with a centrifuge, soaked in isopropanol and fully stirred after being separated;
[0034] (5) Separate the nano-titanium dioxide particles from the solution obtained in step (4) by a centrifuge again, soak them in water after separation, repeat this step 3 times, and ...
Embodiment 2
[0047] Preparation of nano-titanium dioxide sol:
[0048] (1) Mix 30 parts by mass of isopropanol with 50 parts by mass of deionized water, add sulfuric acid, control its concentration to be 0.4mol / L, and stir for 3 minutes;
[0049] (2) Add n-butyl titanate to the above solution, control its concentration to 0.2 mol / L, adjust the pH between 2 and 4, continue stirring for 20 minutes, and record the mixed solution as C solution;
[0050] (3) Mix 30 parts by mass of potassium fluotitanate and 70 parts by mass of absolute ethanol, add the mixed solution into the C solution, control the addition rate to 2ml / min, and stir for 2 hours;
[0051] (4) The nano-titanium dioxide particles obtained in step (3) are separated with a centrifuge, soaked in isopropanol and fully stirred after being separated;
[0052] (5) Separate the nano-titanium dioxide particles from the solution obtained in step (4) by a centrifuge again, soak them in water after separation, repeat this step 3 times, and...
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