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118 results about "Ethylene glycol diethyl ether" patented technology

Ethylene glycol dimethyl ether (dimethoxyethane, CH3OCH2CH2OCH3), a higher boiling alternative to diethyl ether and THF, also used as a solvent for polysaccharides, a reagent in organometallic chemistry and in some electrolytes of lithium batteries.

Nanometer polysiloxane nontoxic low-surface-energy ship antifouling coating and preparation method thereof

The invention relates to the field ship antifouling coatings, in particular to a nanometer polysiloxane nontoxic low-surface-energy ship antifouling coating for sea ships and a preparation method thereof, which are used for solving the problem of long-term nontoxicity, antifouling and corrosion on the outer bottom surface of a ship. The nanometer polysiloxane nontoxic low-surface-energy ship antifouling coating comprises the following components in parts by weight: 50-55 parts of polysiloxane resin, 1-5 parts of nanometer slurry, 5-8 parts of dimethylbenzene, 6-10 parts of butyl ester; 2.0-3.0 parts of ethylene glycol diethyl ether acetic ester, 0.3-0.5 part of a dispersing agent, 0.3-0.5 part of an antifoaming agent, 0.1-0.3 part of a flatting agent, 0.5-0.8 part of an anti-settling agent, 0.4-0.7 part of gas phase white carbon black, 15-22 parts of a pigment and 3-6 parts of a filler. The preparation method comprises the following steps of: proportionally preparing, dispersing, and grinding till the fineness is below 30 micros to obtain a component A; and mixing the component A and the component B for curing to obtain the nontoxic long-term ship sea antifouling coating. The nanometer polysiloxane nontoxic low-surface-energy ship antifouling coating is a surface protection material with extreme low surface energy, and plays roles in preventing fouling and scaling, and marine organisms are prevented from being adhered to the antifouling coating easily.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI +1

Organic phase electrolyte and application thereof in negative electrode of redox flow battery

The invention discloses an organic phase electrolyte and an application thereof in a negative electrode of a redox flow battery. The organic phase electrolyte consists of active materials, a supporting electrolyte and an organic solvent, wherein the active materials are diphenyl ketone and a derivative thereof, anthrone and a derivative thereof, or dibenzoyl methane and a derivative thereof; the supporting electrolyte is selected from tetraethylammonium hexafluorophosphate, tetraethylammonium tetrafluoroborate, tetrabutylammonium hexafluorophosphate or tetrabutylammonium tetrafluoroborate; and the organic solvent is selected from acetonitrile, tetrahydrofuran, propylene carbonate, ethylene carbonate, dimethyl sulfoxide, dimethylformamide, glycol dimethyl ether or ethylene glycol diethyl ether. The organic phase electrolyte disclosed by the invention has relatively low electrochemical potential and high electrochemical property; when the organic phase electrolyte is used as the negative electrode electrolyte of the redox flow battery for assembling an organic phase redox flow battery, relatively high open-circuit voltage can be realized, so that the energy density of the battery can be improved; and meanwhile, the capacity fading of the battery can be lowered, so that the cycle life of the battery can be prolonged.
Owner:TIANJIN UNIV

Method for directly co-preparing glycol dimethyl ether and ethylene glycol from ethylene glycol monomethyl ether

The invention provides a method for directly co-preparing glycol dimethyl ether and ethylene glycol from ethylene glycol monomethyl ether. The method specifically comprises the following steps: enabling a raw material ethylene glycol monomethyl ether and optional inert gas which is taken as carrier gas to pass through a reactor loaded with a solid acid catalyst; reacting under conditions with a reaction temperature ranging from 40 DEG C to 150 DEG C and reaction pressure ranging from 0.1 Mpa to 15.0 Mpa to generate glycol dimethyl ether and ethylene glycol, wherein mass space velocity of the raw material ethylene glycol monomethyl ether ranges from 0.05 h<-1> to 5.0 h<-1>; and volume concentration of the raw material ethylene glycol monomethyl ether is 1-100%, and volume concentration of the carrier gas is 0-99%. Under a low-temperature condition, the method takes solid acid as a catalyst and takes ethylene glycol monomethyl ether as the raw material to prepare glycol dimethyl ether and ethylene glycol with high selectivity; and meanwhile, formation of a byproduct 1,4-dioxane which pollutes the environment or damages a human body or an animal body is basically or completely avoided.
Owner:DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Preparation and application of printing and dyeing sewage treatment agent

The invention discloses preparation and application of a printing and dyeing sewage treatment agent. The preparation steps are follows: adding a coconut shell powder into a phosphoric acid solution for soaking, calcinating for activation, and then adding a copper nitrate solution and an yttrium nitrate solution for modification, and calcinating to obtain modified coconut shell activated carbon; adding an organic modifier and aluminum chloride into deionized water, then adding bentonite, reacting, and grinding to obtain modified bentonite; taking modified coconut shell activated carbon powder,polymeric ferric trichloride, polyaluminum chloride, modified bentonite, corn starch, sodium acetate, polyacrylamide, polysorbate, plant fiber and ethylene glycol-bis(beta-aminoethyl ether)-N,N,N',N'-tetraacetic acid, uniformly mixing, and granulating to obtain the sewage treatment agent. The invention has the beneficial effects as follows: by the preparation method, raw materials are compounded to play a coordinated role, and printing and dyeing sewage with relatively high chroma and concentration can be continuously treated, and the treated water can be reused repeatedly; a technology for treating the dyeing and dyeing sewage by using the water treatment agent is simple, efficient, low in treatment cost and free of side effects on operators.
Owner:ZHEJIANG OCEAN UNIV

Biomass chelated modified heavy metal capturing agent as well as preparation method and application thereof

The invention relates to a biomass chelated modified heavy metal capturing agent as well as a preparation method and application thereof. The biomass chelated modified heavy metal capturing agent is characterized by being prepared from konjac glucomannan, water, an initiator azobis(2-methylpropionamidine)dihydrochloride V-50, N-vinylformamide, ethylene glycol-bis-(2-aminoethylether)-N,N,N',N'-tetraacetic dianhydride, potassium hydroxide and carbon disulfide; the biomass chelated modified heavy metal capturing agent is used for treating heavy-metal wastewater discharged by electroplating, smelting, mining, mineral dressing, chemical industry, machines and the like. According to the biomass chelated modified heavy metal capturing agent, complex heavy metal ions can be adsorbed through a synthesized konjac glucomannan macromolecular framework grafted novel chelated functional group; each basic unit can provide hexa-coordinate atoms to carry out strong chelating and adsorption; furthermore, sodium dithiocarbamate of a konjac glucomannan grafted sedimentation-assisting side chain and a sedimentation-assisting agent are subjected to chemical sedimentation reaction and a large aggregate is generated within a few of seconds, so that rapid sedimentation is realized.
Owner:合肥九州龙腾科技成果转化有限公司

Solvent method synthetic process of Si-75

InactiveCN104804032AHigh purityOvercoming steric potentialGroup 4/14 element organic compoundsDistillationImpurity
The invention relates to a solvent method synthetic process of Si-75. Si-75 can be used for radial tyres and other rubber products and belongs to the technical field of coupling agents. The solvent method synthetic process comprises the following steps: adding sodium sulfide containing nine crystal water and powdered sulfur into methylbenzene, heating, dewatering, cooling, adding gamma-chloropropyl triethoxysilane and absolute ethyl alcohol, then adding ethylene glycol diethyl ether, heating, after the reaction, cooling to the room temperature, filtering inorganic salt and impurities for industrial salt application, transferring filtrate to a distiller, distilling solvent and foreshot under reduced pressure for recycling, and performing distillation to obtain the Si-75 when the vacuum degree is greater than or equal to 0.090 Mpa and the temperature is greater than or equal to 150 DEG C, wherein the molar ratio of the sodium sulfide to the powdered sulfur is 1:1, the weight ratio of the methylbenzene to the sodium sulfide is 1.6-2, the weight ratio of the gamma-chloropropyl triethoxysilane to the sodium sulfide is 2.00-2.06, the weight ratio of the absolute ethyl alcohol to the absolute ethyl alcohol is 1:1, and the weight ratio of the ethylene glycol diethyl ether to the methylbenzene is 0.3-0.6.
Owner:NANCHANG GANYU ORGANOSILICONE

Preparation and applications of aquatic product sewage treatment agent

The invention discloses a preparation method and applications of an aquatic product sewage treatment agent. The preparation method comprises following steps: mussel shell is treated with a diluted acid solution, and then is subjected to high temperature treatment and grinding so as to obtain mussel shell powder; an organic modifying agent and aluminium chloride are dissolved with deionized water,roasted bentonite is added, and stirring, reaction, and grinding are carried out so as to obtain modified bentonite; the mussel shell powder, sodium alginate, polyferric chloride, polymeric aluminium,the modified bentonite, polyacrylamide, vegetable fiber, and ethylene glycol-bis-(2-aminoethylether)-N,N, N', N'-tetraacetic acid (EGTA) are uniformly mixed, are subjected to pelletizing moulding ina pelletizer, and are dried so as to obtain the aquatic product sewage treatment agent. The beneficial effects are that: the advantages of the ingredients are achieved, synergetic effects are achieved, nitrogen, phosphor, and organic pollutants can be removed effectively, the aquatic product sewage treatment agent can be recycled, and can be used for aquatic product sewage treatment, the treatmenttechnology is simple, the operationality is high, efficiency is high, and no side effect on operation personnel is caused .
Owner:江苏金山新材料科技有限公司
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