Preparation method of hollow fiber composite loose nanofiltration membrane
A fiber composite and nanofiltration membrane technology, applied in spinning solution preparation, chemical instruments and methods, membranes, etc., can solve the problems of large pollution, stench, sensory pollution, etc. Effect of small size and small separation aperture
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[0028] (1) Preparation of polyethersulfone casting solution:
[0029] According to the proportion by weight: the mass ratio of polyethersulfone: dimethylacetamide: polyethylene glycol is 34:50:16 and mixed in the stirring tank, stirring and dissolving in the stirring tank at a temperature of 65°C for 12 hours ; The polyethersulfone casting solution obtained by stirring and dissolving is transferred to the spinning storage tank, and the polyethersulfone spinning casting solution is obtained by standing at a temperature of 65° C. for defoaming and aging.
[0030] (2) Preparation of polyethersulfone hollow fiber nanofiltration membrane:
[0031] The pressure of 0.2MPa is provided by the nitrogen cylinder, so that the casting liquid passes through the flow-controllable feed metering pump, enters the spinneret at a flow rate of 15mL / min, and is sprayed vertically downward under the action of the core liquid at a flow rate of 5mL / min. out. After passing through a 40cm air bath, th...
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