Preparation method of TiO2/diatomite composite material
A technology of composite materials and diatomite, applied in chemical instruments and methods, water/sludge/sewage treatment, chemical/physical processes, etc., to achieve the effects of improving catalytic efficiency, stable product quality, and easy operation
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Embodiment 1
[0037] Embodiment 1 (mode 1)
[0038] See attached figure 1 , a kind of TiO provided by the present invention 2 The preparation method of / diatomite composite material specifically comprises the following steps:
[0039] (1) Mix 20mL of butyl titanate, 50mL of absolute ethanol, and 1mL of glacial acetic acid to make liquid A, and set aside;
[0040] (2) Mix 20mL of absolute ethanol and 4mL of glacial acetic acid evenly to make liquid B, set aside;
[0041] (3) At a stirring rate of 2000r / min, slowly drop the liquid B obtained in step (2) into the liquid A obtained in step (1) to obtain a uniform transparent solution;
[0042] (4) Place the homogeneous transparent solution obtained in step (3) at room temperature and age for 48 hours;
[0043] (5) After diluting the aging-treated solution in step (4) to 200mL, place it in the magnetic stirring device of a small spray dryer for stirring;
[0044] (6) Set the spray temperature to 95° C., and the air flow rate to 1000 L / h, and...
Embodiment 2
[0054] Embodiment 2 (mode 2)
[0055] See attached figure 2 , another TiO provided by the present invention 2 The preparation method of / diatomite composite material specifically comprises the following steps:
[0056] (1) Mix 20mL of butyl titanate, 50mL of absolute ethanol, and 1mL of glacial acetic acid to make liquid A, and set aside;
[0057] (2) Mix 20mL of absolute ethanol and 4mL of glacial acetic acid evenly to make liquid B, set aside;
[0058] (3) At a stirring rate of 2000r / min, slowly drop the liquid B obtained in step (2) into the liquid A obtained in step (1) to obtain a uniform transparent solution;
[0059] (4) Place the homogeneous transparent solution obtained in step (3) at room temperature and age for 48 hours;
[0060] (5) After diluting the aging-treated solution in step (4) to 200mL, place it in the magnetic stirring device of a small spray dryer for stirring;
[0061] (6) Set the spray temperature to 95° C., and the air flow rate to 1000 L / h, and ...
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