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A Multi-bed Axial Radial Reactor

An axial-radial, reactor technology, applied in chemical instruments and methods, chemical/physical processes, etc., can solve the problems of obvious amplification effect, high production capacity, small pressure drop in the bed, etc., to avoid gas bias flow and ensure stable The effect of running, avoiding the reaction dead zone

Active Publication Date: 2019-05-10
SINOPEC ENG +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The axial fixed bed reactor design, processing process is relatively easy, and the operation is simple, but there are problems such as large size of reactor equipment, large bed pressure drop, prone to partial temperature runaway, slow heat transfer, low conversion rate, and obvious amplification effect.
The radial bed reactor has the advantages of large height-to-diameter ratio, small bed pressure drop, short residence time of reactants in the catalyst bed, low operating cost, high production capacity, can use small particle catalysts, and is easy to scale up. Achieve uniform distribution of reactants in the radial direction

Method used

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  • A Multi-bed Axial Radial Reactor
  • A Multi-bed Axial Radial Reactor
  • A Multi-bed Axial Radial Reactor

Examples

Experimental program
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Effect test

Embodiment 1

[0049] Such as figure 1 As shown, the multi-bed axial radial reactor used in this embodiment includes a cylindrical sealed pressure-bearing shell 2, an air inlet pipe 16 extending from the top of the shell 2 into the inside of the shell, and is arranged in the shell 2 The axis coaxial with the casing 2 below the inlet pipe 16 is radial to the catalytic reaction zone 8 and the outlet pipe 14 . The upper part of the intake pipe 16 has an air inlet 1 , the lower part is provided with a first gas distributor 3 , and the lower part of the first gas distributor 3 is provided with a second gas distributor 4 . The catalytic reaction zone 8 in the radial direction of the axis is a cylindrical accommodation space that can accommodate the catalyst bed. The outer shell of the accommodation space is formed by a side wall 11, a top cover 5 and a bottom cover 18. The top cover 5 is a spherical head, and the side wall 11 and the back cover 18 have a perforated structure, and the back cover 1...

Embodiment 2

[0056] Such as image 3 , Figure 4 As shown, the reactor of this embodiment is the same as the reactor shell inner diameter, the height of the catalytic reaction zone, the opening and other structural parameters of the reactor in embodiment 1. The difference from Example 1 is that no partition is set in the reactor of this example. The reactor of this embodiment can also be used for methanation reaction. The process conditions adopted in Example 1 are the same.

[0057] From the perspective of the temperature distribution of the catalyst bed, the average distance between the hot spot position of the bed and the side wall 11 is 255mm, and the hot spot value is 923K. Table 2 shows the comparison between the multi-bed axial radial reactor in this embodiment and the radial reactor in the prior art. Likewise, both reactors had the same catalyst loading. It can be seen from the three indicators of bed layer uniformity, hot spot position and CO conversion rate that the reactor ...

Embodiment 3

[0061] Such as Figure 5 , Figure 6 As shown, the reactor of this embodiment is the same as the reactor shell inner diameter, the height of the catalytic reaction zone, the opening and other structural parameters of the reactor in embodiment 1. The difference from Example 1 is that no gas redistribution plate is provided in the reactor of this example, and the number of partitions is 9, and the angle between adjacent partitions is 40°. The reactor of this embodiment can also be used for methanation reaction. The process conditions adopted in Example 1 are the same.

[0062] From the perspective of the temperature distribution of the catalyst bed, the average distance between the hot spot position of the bed and the side wall 11 is 257mm, and the hot spot value is 923K. Table 3 shows the comparison between the multi-bed axial radial reactor used in this example and the radial reactor in the prior art. Likewise, both reactors had the same catalyst loading. It can be seen f...

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Abstract

The invention discloses a multi-bed axial and radial reactor. The reactor comprises a radial cylindrical sealed pressure-bearing shell (2), an air inlet pipe (16), an axial-radial catalytic reaction zone (8) and an air outlet pipe (14), wherein the axial-radial catalytic reaction zone (8) is a cylindrical containing space capable of containing catalyst beds; the containing space is formed by side walls (11), a top seal head (5) and a seal bottom (18); the side walls (11) and the alternative seal bottom (18) are of an opening structure through which fluid can penetrate but solid catalysts cannot penetrate; and the top seal head (5) is of a fluid impenetrable structure. The pressure of the reactor is reduced, the space utilization rate is high, and any gas flow deviation or short-circuit phenomenon is avoided.

Description

technical field [0001] The invention relates to a multi-bed axial radial reactor. Background technique [0002] There are mainly two types of fixed bed reactors, one is axial fixed bed reactor and the other is radial fixed bed reactor. The axial fixed bed reactor is relatively easy to design and process, and simple to operate, but there are problems such as large size of reactor equipment, large pressure drop in the bed layer, prone to local temperature jump, slow heat transfer, low conversion rate, and obvious amplification effect. The radial bed reactor has the advantages of large height-to-diameter ratio, small bed pressure drop, short residence time of reactants in the catalyst bed, low operating cost, high production capacity, can use small particle catalysts, and is easy to scale up. To achieve uniform distribution of reactants in the radial direction. [0003] The advantages and disadvantages of radial bed reactor design have a great influence on the reaction proces...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J8/04
CPCB01J8/008B01J8/04B01J8/0492B01J2208/00938B01J2208/027
Inventor 张旭智凯敏张奇戴文松蒋荣兴
Owner SINOPEC ENG
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